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0343504199
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note
-
The most intense peaks corresponded to the protonated azacrown (m/z = 264.2) and to the uncomplexed protonated hosts (m/z = 699.4), showing that under the FAB+ conditions, even the uncomplexed hosts are relatively unstable.
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25
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0343504194
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0343504193
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note
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3OD did not show the singlet at 8.8 ppm of the picrate nor any signal belonging to the amine.
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