Monitoring pH swing crystallization of nicotinic acid by the use of attenuated total reflection Fourier transform infrared spectrometry

Industrial and Engineering Chemistry Research

Volumn 39, Issue 6, 2000, Pages 2101-2104

  Wang, Fang ^a,b   Berglund, Kris A ^a,b,c  

^a MICHIGAN STATE UNIVERSITY   (United States)

^b Michigan State University   (United States)

^c Michigan State University   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

FOURIER TRANSFORM INFRARED SPECTROSCOPY; HYDROCHLORIC ACID; LEAST SQUARES APPROXIMATIONS; PH; SOLUBILITY; SUPERSATURATION;

AQUEOUS MIXTURES; NICOTINIC ACID;

CRYSTALLIZATION;

DESICCANT; NICOTINIC ACID;

AQUEOUS SOLUTION; ARTICLE; COOLING; CRYSTALLIZATION; DATA ANALYSIS; FILTRATION; INFRARED SPECTROMETRY; PH; PROTON TRANSPORT; SOLUBILITY;

EID: 0034130446     PISSN: 08885885     EISSN: None     Source Type: Journal    
DOI: 10.1021/ie9901426     Document Type: Article

References (11)

1. Dunuwila, D. D. An Investigation of the Feasibility of Using In Situ ATR-FTIR Spectroscopy in the Measurement of Crystallization Phenomena for Research and Development of Batch Crystallization Process. Ph.D. Dissertation, Michigan State University, East Lansing, MI, 1996.
2. Uusi-Pentilä, S. M. Optimization of Batch Anti-solvent Crystallization. Ph.D. Dissertation, Michigan State University, East Lansing, MI, 1997.
3. ASI Applied Systems. ReactIR 1000 User's Guide, 3rd ed.; ASI Applied Systems: Millersville, MD, 1997.
4. Nakamoto, K.; Morimoto, Y.; Martell, A. E. Infrared Spectra of Aqueous Solutions. III. Ethylenediaminetetraacetic Acid, N-Hydroxyethylenediaminetriacetic Acid and Diethylenetriaminepentaacetic Acid. J. Am. Chem. Soc. 1963, 85, 309.
5. Wojcik, J. F.; Stock, T. H. Aqueous Infrared Studies of the Pyridine Carboxylic Acids. J. Phys. Chem. 1969, 73 (7), 2153.
6. Colthup, N. B.; Daly, L. H.; Wiberley, S. E. Introduction to Infrared and Raman Spectroscopy, 3rd ed.; Academic Press: Boston, 1990.
7. Cohn, E. J.; Edsall, J. G. Proteins, Amino Acids and Peptides as Ions and Dipolar Ions; Waverly Press: New York, 1943.
8. Beebe, K. R.; Kowalski, B. R. An Introduction to Multivariate Calibration and Analysis. Anal. Chem. 1987, 59 (17), 1017A.
9. Esbensen, K.; Schönkopf, S.; Mictgaard, T. Multivariate Analysis in Practice; Computer-aided modelling AS: Trondheim, Norway, 1996.
10. Green, R. W.; Tong, H. K. The Constitution of the Pyridine Monocarboxylic Acids in their Isoelectric Forms. J. Am. Chem. Soc. 1956, 78, 4896.
11. Mullin, J. W. Crystallization, 3rd ed.; Butterworth-Heinemann Ltd.: Oxford, 1993.