Chemical derivatization and the selection of deuterated internal standard for quantitative determination - Methamphetamine example

Journal of Analytical Toxicology

Volumn 24, Issue 4, 2000, Pages 275-280

  Lin, Dong Liang ^a   Chang, Wei Tun ^b   Kuo, Tsung Li ^c   Liu, Ray H ^d  

^a Min of Justice Investigation Bureau   (Taiwan)

^b CENTRAL POLICE UNIVERSITY   (Taiwan)

^c NATIONAL TAIWAN UNIVERSITY   (Taiwan)

^d UNIVERSITY OF ALABAMA AT BIRMINGHAM   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

METHAMPHETAMINE;

ARTICLE; CHEMICAL STRUCTURE; CONTROLLED STUDY; DRUG DETERMINATION; EXTRACTION; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; STANDARD;

EID: 0034118057     PISSN: 01464760     EISSN: None     Source Type: Journal    
DOI: 10.1093/jat/24.4.275     Document Type: Article

References (12)

1. U.S. Department of Health and Human Services (Substance Abuse and Mental Health Services Administration). Mandatory guidelines for federal workplace drug testing programs. Fed. Regist. 59: 29916-29931 (1994).
2. R. Kronstrand, S. Förstberg-Peterson, B. Kågedal, J. Ahlner, and G. Larson. Codeine concentration in hair after oral administration is dependent on melanin content. Clin. Chem. 45: 1485-1494 (1999).
3. T. Mieczkowski and R. Newel. A evaluation of patterns of racial bias in hair assays for cocaine: black and white arrestees compared. Forensic Sci. Int. 63: 85-98 (1993).
4. G. Skopp, L. Pötsch, and M.R. Moeller. On cosmetically treated hair - aspects and pitfalls of interpretation. Forensic Sci. Int. 84: 43-52 (1997).
5. V. Cirimele, P. Kintz, and P. Mangin. Drug concentration in human hair after bleaching. J. Anal. Toxicol. 19: 331-332 (1995).
6. S. Valtier and J.T. Cody. Evaluation of internal standards for the analysis of amphetamine and methamphetamine. J. Anal. Toxicol. 19: 375-380 (1995).
7. F.M. Urry, M. Kushnir, G. Nelson, M. McDowell, and T. Jennison. Improving ion mass ratio performance at low concentrations in methamphetamine GC-MS assay through internal standard selection. J. Anal. Toxicol. 20: 592-595 (1996).
8. R.H. Liu, L.D. Baugh, E.E. Allen, S.C. Salud, J.C. Fentress, H. Chadha, and A.S. Walia. Isotopic analogue as the international standard for quantitative determination of benzoylecgonine: concerns with isotopic purity and concentration level. J. Forensic Sci. 34: 986-990 (1989).
9. R.H. Liu, G.F. Foster, E.J. Cone, and S.D. Kumar. Selecting an appropriate isotopic internal standard for gas chromatography/mass spectrometry analysis of drugs of abuse - pentobarbital example. J. Forensic Sci. 40: 983-989 (1995).
10. 5 (side chain) as an internal standard. J. Food Drug Analysis (Taipei). 4: 123-130 (1996).
11. C.L. Hornbeck and R.J. Czarny. Quantitation of methamphetamine and amphetamine in urine by capillary GC/MS. Part I. Advantages of trichloroacetyl derivatization. J. Anal. Toxicol. 13:144-149 (1989).
12. 4-Secobarbital as the internal standard for the quantitative determination of secobarbital - a critical evaluation. J. Forensic Sci. 45: 659-664 (2000).