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0001373911
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0004374396
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Marko, I.E.1
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14
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0343818681
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-
note
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4 were used to convert olefins 11 to diols 12.
-
-
-
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15
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33845469398
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(a) Hauser, F.M.; Ellenberger, S.R.; Clardy, J.C.; Bass, L.S. J. Am. Chem. Soc. 1984, 106, 2458.
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18
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0028292023
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For instances in which S oxidation is not observed under catalytic conditions; see: (a) Walsh, P.J.; Ho, P.T.; King, S.B.; Sharpless, K.B. Tetrahedron Lett. 1994, 35, 5129;
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Walsh, P.J.1
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19
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0028954582
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(b) Eames, J.; Mitchell, H.J., Nelson, A.; O'Brian, P.; Warren, S.; Wyatt, P. Tetrahedron Lett. 1995, 36, 1719.
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0012989810
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21
-
-
0342513438
-
-
note
-
Partial product degradation was observed when the sodium sulfite wash was included in the reaction protocol.
-
-
-
-
22
-
-
0343818680
-
-
note
-
+), 185, 157.
-
-
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23
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0000058108
-
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By analogy to: Ichikawa, Y.; Isobe, M.; Konobe, M.; Goto, T. Carbohydr. Res. 1987, 171, 193.
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24
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0001493681
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Zhai, D.; Zhai, W.; Williams, R.M. J. Am. Chem. Soc. 1988, 110, 2501.
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Zhai, D.1
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26
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24444460116
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For instance: (a) Müller, S.; Liepold, B.; Roth, G.J.; Bestmann, H.J. Synlett 1996, 522.
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Müller, S.1
Liepold, B.2
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29
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0001557673
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(b) Vedejs, E.; Eberlein, T.H.; Wilde, R.G. J. Org. Chem. 1988, 53, 2220.
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Vedejs, E.1
Eberlein, T.H.2
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30
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0000553399
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(d) Vedejs, E.; Stults, J.S.; Wilde, R.G. J. Am. Chem. Soc. 1988, 110, 5452.
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31
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33748398527
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(c) Vedejs, E.; Eberlein, T.H.; Varie, D.L. J. Am. Chem. Soc. 1982, 104, 1445.
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Vedejs, E.1
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32
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33845374421
-
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(e) Vedejs, E.; Eberlein, T.H.; Mazur, D.J.; McClure, C.K.; Perry, D.A.; Ruggeri, R.; Schwartz, E.; Stults, J.S.; Varie, D.L.; Wilde, R.G.; Wittenberger, S. J. Org. Chem. 1986, 51, 1556.
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Wilde, R.G.10
Wittenberger, S.11
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35
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0013631701
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(b) Morita, H.; Takeda, M.; Fujii, T.; Yoshimura, T.; Shimasaki, C. J. Org. Chem. 1997, 62, 9018.
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Shimasaki, C.5
-
39
-
-
0000296710
-
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(f) For a theoretical treatment, see: Barone, V.; Arnaud, R.; Chavant, P.Y.; Vallée, Y. J. Org. Chem. 1996, 61, 5121.
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Barone, V.1
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Vallée, Y.4
-
41
-
-
0342513435
-
-
note
-
As compound 20 was stable in toluene at 110 °C, all other experiments were carried out under these conditions.
-
-
-
-
45
-
-
0343818677
-
-
note
-
2, r.t., 95%, v) conditions iii).
-
-
-
-
46
-
-
0342513434
-
-
note
-
2O, -30 °C, 1-2 h, 91%].
-
-
-
-
47
-
-
0343383025
-
-
note
-
In certain experiments minor quantities of the C-2 epimeric 29 were also isolated.
-
-
-
-
48
-
-
0342947554
-
-
note
-
13C NMR spectra for compounds 28 and 29. However, from the 2D C-H and COSY spectra, the identity of the C-2 and C-3 centers was established, along with the 2,3-relative stereochemistry. (matrix presented)
-
-
-
-
49
-
-
0343818676
-
-
note
-
2, -78 °C, 85%, iii) NaH, BnBr, THF, 94%, iv) steps ii-iv in Ref 21, v) NaH, TBSCI, THF, 0 °C, 1 h.
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