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23), the MALDI-TOF spectrum features a signal at around m/z = 2950 pointing to possible dimer formation in the gas phase as well.
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The solubility at room temperature was determined by UV measurements using a soluble tetrakis(bromomethyl)cavitand of comparable molecular weight as a standard. The solubility of 6 corresponds to less than 0.5 mM in chloroform.
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50
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