Optimization of separation of methamphetamine enantiomers by capillary GC/MS

Japanese Journal of Forensic Toxicology

Volumn 18, Issue 1, 2000, Pages 21-31

  Amemiya, Masayoshi ^a,c   Rai, Tatenaka ^a   Nagai, Tatsuo ^b,c  

^a Forensic Science Laboratory   (Japan)

^b KITASATO UNIVERSITY SCHOOL OF MEDICINE   (Japan)

^c KITASATO UNIVERSITY   (Japan)

Author keywords

Amphetamine; Chiral column; Enantiomers; GC MS; Methamphetamine; Optical isomers

Indexed keywords

AMPHETAMINE; METHAMPHETAMINE;

ANALYTIC METHOD; ARTICLE; CAPILLARY GAS CHROMATOGRAPHY; CHIRALITY; DERIVATIZATION; ENANTIOMER; ION PAIR CHROMATOGRAPHY; ISOMER; MASS SPECTROMETRY; PHASE SEPARATION; RADIOIMMUNOASSAY;

EID: 0034062218     PISSN: 09159606     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (18)

1. Suzuki, S., Inoue, T., Hori, H. and Inayama, S.: Analysis of methamphetamine in hair, nail, sweat, and saliva by mass fragmentography. J Anal Toxicol, 13, 176-178 (1989).
2. Rasmussen, S., Cole, R. and Spiehler, V.: Methamphetamine in antemortem blood and urine by radioimmunoassay and GC/ MS. J Anal Toxicol, 13, 263-267 (1989).
3. Nagai, T., Nagai, T. and Ikeda, T.: Study on the drug abuse in forensic science detection of methamphetamine and amphetamine from hair, bone and teeth. In Dunnett. N. and Kimber, K.J. (eds), Proceedings of the 21st International TIAFT Meeting, Brighton, 1984, pp. 89-91.
4. Derk E.A.: Procedure for the differentiation of the optical isomers of amphetamine and methamphetamine by thin-layer chromatography. J Chromatogr, 117, 442-444 (1976).
5. Kalasinsky, K. S., Levine, B., Smith, M. L., Magluilo, J., Jr. and Schaefer, T.: Detection of amphetamine and methamphetamine in urine by gas chromatography/ Fourier transform infrared (GC/FTIR) spectoroscopy. J Anal Toxicol, 17, 359-364 (1993).
6. Peyton J., III, Tisdale, E.C., Panganiban, K., Cannon, D., Zabel, K., Mendelson, J.E. and Reese, T.J.: Gas chromatographic determination of methamphetamine and its metabolite amphetamine in human plasma and urine following conversion to N-propyl derivatives. J Chromatogr B, 664, 449-457 (1995).
7. Makino, Y., Ohta, S. and Hirobe, M.: Enantiomeric separation of amphetamine by high-performance liquid chromatography using chiral crown ether-coated reversed-phase packing: application to forensic analysis. Forensic Sci Int, 78, 65-70 (1996).
8. Nagai, T., Kamiyama, S. and Nagai, T.: Forensic toxicologic analysis of methamphetamine and amphetamine optical isomers by high performance liquid chromatography. Z Rechtsmed, 101, 151-159 (1988).
9. Hornbeck, C.L. and Czarny, R.J.: Quantitation of methamphetamine and amphetamine in urine by capillary GC/MS, Part I . Advantages of trichloroacetyl derivatization. J Anal Toxicol, 13, 144-149 (1989).
10. Ilonka B.V. Craige T. and Pieter S.: Separation and quantitation of optical isomers of methylamphetamine samples by capillary electrophoresis. Forensic Sci Int, 85, 177-192 (1997).
11. Sato, M., Arakida, Y. and Ushio, Y.: Separation of optical isomers of methamphetamine by capillary electrophoresis. Jpn J Forensic Toxicol, 14, 52-57 (1996).
12. Tarjanyi, Zs., Kalász, H., Szebeni, G., Hollósi, I., Báthori, M. and Fürst S.: Gas-chromatographic study on the stereoselectivity of deprenyl metabolism. J Pharm Biomed Anal, 17, 725-731 (1998).
13. Meeker, J. E. and Reynolds, P. C.: Postmortem tissue methamphetamine concentrations following selegiline administration. J Anal Toxicol, 14, 330-331 (1993).
14. Ho-Sang, S.: Metabolism of selegiline in humans. Identification, excretion, and stereochemistry of urine metabolites. Drug Metab and Dispos, 25, 657-662 (1997).
15. Cody, J. T. and Schwarzhoff, R.: Interpretation of methamphetamine and amphetamine enantiomer data. J Anal Toxicol, 17, 321-326 (1993).