Methods for ELNES-quantification: Characterization of the degree of inversion of Mg-Al-spinels

Micron

Volumn 31, Issue 4, 2000, Pages 347-354

  van Benthem, K ^a   Kohl, H ^a  

^a UNIVERSITY OF MÜNSTER   (Germany)

Author keywords

Degree of inversion; Electron energy loss spectroscopy; Energy loss near edge structures; Mg Al spinel; Multiple scattering calculations; Quantification

Indexed keywords

EID: 0034058086     PISSN: 09684328     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0968-4328(99)00113-4     Document Type: Article

References (21)

1. Aebi P., Erbudak M., Vanini F., Vvedensky D.D., Kostorz G. Nondipole channels in the electron-energy-loss structure near the 3s edge of copper. Phys. Rev. B. 42:1990;5369-5372.
2. Bruley J., Tseng Ming-Wei, Williams D.B. Spectrum-line profile analysis of a magnesium aluminate spinel/sapphire interface. Microsc. Microanal. Microstruct. 6:1995;1-18.
3. Brydson R., Sauer H., Engel W., Thomas J.M., Zeitler E. Coordination fingerprints in electron loss near-edge structures: Determination of the local site symmetry of aluminium and beryllium in ultrafine minerals. J. Chem. Soc., Chem. Commun. 15:1989;1010-1012.
4. Brydson R. Interpretation of near-edge structure in the electron energy-loss spectrum. EMSA Bull. 21:1991;57-67.
5. Brydson R., Sauer H., Engel W. Disko M.M., Ahn C.C., Fulz B. Transmission electron energy loss spectroscopy in materials science. TMS Tomograph Series, Warrendale, USA. 1992;131-154.
6. Brydson R., Brown L.M., Bruley J. Characterizing the local nitrogen enviroment at platelets in type IaA/B diamond. J. Microsc. 189:1998;137-137.
7. Davoli I., Marcelli A., Bianconi A., Tomellini M., Fanfoni M. Multielectron configurations in the X-ray-absorption near-edge structure on NiO at the oxygen K threshold. Phys. Rev. B. 33:1986;2979-2982.
8. Durham P.J., Pendry J.B., Hodges C.H. Calculation of X-ray absorption near-edge structure. XANES, Comput. Phys. Commun. 25:1982;193-205.
9. Egerton R.F. Electron energy loss spectroscopy in the electron microscope. 2:1996;Plenum, New York.
10. Harris V.G., Williams C.G., Abe M., Zhang Q. Multiple-scattering extended X-ray absorption fine structure analysis of spinel ferrites: cation site distribution in NiZn-ferrite films. J. Physique IV. 7:1997.
11. McCulloch D.G., Brydson R. Carbon K-shell near-edge structure calculations for graphite using the multiple-scattering approach. J. Phys. Condens. Matter. 8:1996;3835-3841.
12. Putnis, A., 1998. Personal communication.
13. Redfern, S.A.T., Harrison, R.J., O'Neill, Hugh St.C., Wood, D.R.R., 1998. Thermo-dynamics and Kinetics of Cation Ordering in MgAl2O4 Spinel up to 1600°C from in situ Neutron Diffraction. Submitted for publication.
14. Redlich, Ph., 1994. Calculation of X-ray absorption near edge structures (XANES). Unpublished.
15. Redlich Ph., Banhart F., Lyutovich Y., Ajayan P.M. EELS study of the irradiation-induced compression of the carbon onions and their transformation to diamond. Carbon. 36:1998;561-563.
16. Reimer L. Energy Filtering Transmission Electron Microscopy. 1997;Springer, Berlin.
17. van Benthem, K., 1998. Charakterisierung des Inversionsgrades von Mg-Al-Spinellen anhand der kantennahen Feinstrukturen in Elektronen-Energieverlustspektren, Diplomarbeit, Westfälische Wilhelms-Universität Münster. Unpublished.
18. van Benthem K., Wibbelt M., Kohl H. Determination of the degree of inversion of spinels by analysis of the near edge structures in eels. Electron microscopy 1998, Proceedings of ICEM-14, Cancun, Mexico. 14:1998;623-624.
19. Vvedensky D.D., Saldin D.K., Pendry J.B. An update of DLXANES. The calculation of X-ray absorption near-edge structure. Comput. Phys. Commun. 40:1986;421-440.
20. Wibbelt M., Kohl H., Kohler-Redlich Ph. Multiple scattering calculations of electron energy-loss near-edge structures of existing and predicted phases in the ternary system B-C-N. Phys. Rev. 59:1999;739-745.
21. Wyckoff R.M.G. Crystal Structures. II:1964;Wiley, New York.