Achiral and chiral quantification of methamphetamine and amphetamine in human urine by semi-micro column high-performance liquid chromatography and fluorescence

Journal of Forensic Sciences

Volumn 45, Issue 3, 2000, Pages 708-714

  Al Dirbashi, Osama Y ^a   Wada, Mitsuhiro ^a   Kuroda, Naotaka ^a   Takahashi, Masakatsu ^a   Nakashima, Kenichiro ^a  

^a NAGASAKI UNIVERSITY   (Japan)

Author keywords

4(4,5 diphenyl 1H imidazol 2 yl) benzoyl chloride; Achiral and chiral analyses; Fluorescence; Forensic science; Human urine; Methamphetamine; Semi micro column

Indexed keywords

AMPHETAMINE; IMIDAZOLE DERIVATIVE; METHAMPHETAMINE;

ARTICLE; CALIBRATION; CHEMICAL ANALYSIS; CHIRALITY; CONTROLLED STUDY; ELECTRONICS; ENANTIOMER; FLUORESCENCE ANALYSIS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; PRIORITY JOURNAL; QUANTITATIVE ASSAY; TIME; URINALYSIS;

AMPHETAMINE; CENTRAL NERVOUS SYSTEM STIMULANTS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; FLUORESCENCE; FORENSIC MEDICINE; HUMANS; METHAMPHETAMINE; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY;

EID: 0034025656     PISSN: 00221198     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (16)

1. Cho AK Ice: a new dosage form of an old drug. Science 1990;249: 631-4.
2. Reynolds GP, Elsworth JD, Blau K, Sandler M, Lees AJ, Stern GM. Deprenyl is metabolized to methamphetamine and amphetamine in man. Br J Clin Pharmacol 1978;6:542-4.
3. Mei DA, Gross GJ, Nithipatikom K. Simultaneous determination of adenosine, inosine, hypoxanthine, xanthine and uric acid in microdialysis samples using microbore column high-performance liquid chromatography with a diode array detector. Anal Biochem 1996;238:34-9.
4. Tracqui A, Kintz P, Ludes B, Rouge C, Douibi H, Mangin P. High-performance liquid chromatography coupled to ion spray mass spectrometry for the determination of colchicine at ppb levels in human biofluids. J Chromatogr B 1996;675:235-42.
5. Kanazawa H, Nagatsuka T, Miyazaki M, Matsushima Y. Determination of peptides by high-performance liquid chromatography with laser-induced fluorescence detection. J Chromatogr A 1997;763:23-9.
6. Kehr J. Determination of γ-aminobutyric acid in microdialysis samples by microbore column liquid chromatography and fluorescence detection. J Chromatogr B 1998;708:49-54.
7. Kehr J. Determination of glutamate and aspartate in microdialysis samples by reversed-phase column liquid chromatography with fluorescence and electrochemical detection. J Chromatogr B 1998;708:27-38.
8. Parsons LH, Kerr TM, Weiss F. Simple microbore high-performance liquid chromatographic method for the determination of dopamine and cocaine from a single in vivo brain microdialysis sample. J Chromatogr B 1998;709:35-45.
9. Shirota O, Suzuki A, Ohtsu Y, Kimoto S, Makino Y, Ohta S, et al. Direct analysis of methamphetamine in drug abusers' urine by semi-microcolumn high performance liquid chromatography. Chromatography 1996;17:189-93.
10. Suzuki A, Shirota O, Ohtsu Y, Makino Y, Ohta S, Nagano T. Direct analysis of methamphetamine enantiomers in urine by semi-microcolumn liquid chromatography with photodiode array detector: Application to forensic analysis. Chromatography 1997;18:27-30.
11. Al-Dirbashi O, Qvarnstrom J, Irgum K, Nakashima K. Simple and sensitive high-performance liquid chromatographic determination of methamphetamines in human urine as derivatives of 4-(4,5-diphenyl-1H-imidazel-2-yl) benzoyl chloride, a new fluorescence derivatization reagent. J Chromatogr B 1998;712:105-12.
12. Al-Dirbashi O, Kuroda N, Menichini F, Noda S, Minemoto M, Nakashima K. Enantioselective high-performance liquid chromatography with fluorescence detection of methamphetamine and its metabolites in human urine. Analyst 1998;123:2333-7.
13. Al-Dirbashi O, Kuroda N, Inuduka S, Menichini F, Nakashima K. HPLC with fluorescence detection of methamphetamine and amphetamine in segmentally analyzed human hair. Analyst 1999;124:493-9.
14. Nakashima K, Yamasaki H, Kuroda N, Akiyama S. Evaluation of lophine derivatives as chemiluminogens by a flow-injection method. Anal Chim Acta 1995;303:103-7.
15. Katagi M, Nishioka H, Nakajima K, Tsuchihashi H, Fujima H, Wada H, et al. Direct high-performance liquid chromatographic and high-performance liquid chromatographic-thermosepray-mass spectrometric determination of enantiomers of methamphetamine and its main metabolites amphetamine and p-hydroxymethamphetamine in human urine. J Chromatogr B 1996;676:35-43.
16. Hayakawa K, Hasegawa K, Imaizumi N, Wong OS, Miyazaki M. Determination of amphetamine-related compounds by high-performance liquid chromatography with chemiluminescence and fluorescence detections. J Chromatogr 1989;464:34.1-52.