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Volumn 12, Issue 2, 2000, Pages 84-92

Reliable assay of extreme enantiomeric purity values by a new circular dichroism based HPLC detection system

Author keywords

Anisotropy factor; Circular dichroism; Enantiomeric purity; HPLC detection system

Indexed keywords

ANISOTROPY; ARTICLE; CAPILLARY ELECTROPHORESIS; CIRCULAR DICHROISM; ENANTIOMER; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; POLARIMETER; PRIORITY JOURNAL; QUALITY CONTROL; RELIABILITY; STEREOCHEMISTRY;

EID: 0033959516     PISSN: 08990042     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1520-636X(2000)12:2<84::AID-CHIR5>3.0.CO;2-G     Document Type: Article
Times cited : (51)

References (34)
  • 2
    • 0021260726 scopus 로고
    • On chiral drug action
    • Simonyi M. On chiral drug action. Med Res Rev 1984;4:359-413.
    • (1984) Med Res Rev , vol.4 , pp. 359-413
    • Simonyi, M.1
  • 3
    • 0024948937 scopus 로고
    • Enantioselective aspects of drugs action and disposition: Therapeutic pitfalls
    • Jamali J, Mehvar R, Pasutto FM. Enantioselective aspects of drugs action and disposition: therapeutic pitfalls. J Pharm Sci 1989;78:695-715.
    • (1989) J Pharm Sci , vol.78 , pp. 695-715
    • Jamali, J.1    Mehvar, R.2    Pasutto, F.M.3
  • 5
    • 0343067987 scopus 로고
    • The use of circular dichroism as liquid chromatographic detector
    • Brittain HG, Purdie N, editors. Amsterdamn: Elsevier Science
    • Gergely A. The use of circular dichroism as liquid Chromatographic detector. In: Brittain HG, Purdie N, editors. Analytical applications of circular dichroism. Amsterdamn: Elsevier Science; 1994. p 279-292.
    • (1994) Analytical Applications of Circular Dichroism , pp. 279-292
    • Gergely, A.1
  • 6
    • 0040052623 scopus 로고
    • Circular dichroism coupled with HPLC: A powerful tool for analytical, stereochemical and spectroscopic determinations
    • Berova N, Woody RW, Nakanishi K, editors. New York: VCH
    • Salvadori P, Bertucci C, Rosini C. Circular dichroism coupled with HPLC: a powerful tool for analytical, stereochemical and spectroscopic determinations. In: Berova N, Woody RW, Nakanishi K, editors. Circular dichroism: application and interpretation. New York: VCH; 1994. p 541-560.
    • (1994) Circular Dichroism: Application and Interpretation , pp. 541-560
    • Salvadori, P.1    Bertucci, C.2    Rosini, C.3
  • 7
    • 0001286781 scopus 로고
    • Simultaneous monitoring of light absorption and optical activity in the liquid chromatography of chiral substances
    • Drake AF, Gould JM, Mason SF. Simultaneous monitoring of light absorption and optical activity in the liquid chromatography of chiral substances. J Chromatogr 1980;202:239-245.
    • (1980) J Chromatogr , vol.202 , pp. 239-245
    • Drake, A.F.1    Gould, J.M.2    Mason, S.F.3
  • 8
  • 9
    • 0026663784 scopus 로고
    • Chiroptical detection during liquid chromatography: Applications to stereoanalysis and stereodynamics
    • Mannschreck A. Chiroptical detection during liquid chromatography: applications to stereoanalysis and stereodynamics. Chirality 1992;4: 163-169.
    • (1992) Chirality , vol.4 , pp. 163-169
    • Mannschreck, A.1
  • 10
    • 0019047450 scopus 로고
    • Detector based on optical activity for high performance liquid Chromatographic detection of trace organics
    • Yeung ES, Steenhoek LE, Woodruff SD, Kuo JC. Detector based on optical activity for high performance liquid Chromatographic detection of trace organics. Anal Chem 1980;52:1399-1402.
    • (1980) Anal Chem , vol.52 , pp. 1399-1402
    • Yeung, E.S.1    Steenhoek, L.E.2    Woodruff, S.D.3    Kuo, J.C.4
  • 11
    • 0024942039 scopus 로고
    • Polarimetric detection in high-performance liquid chromatography
    • Lloyd DK, Goodall DM. Polarimetric detection in high-performance liquid chromatography. Chirality 1989;1:251-264.
    • (1989) Chirality , vol.1 , pp. 251-264
    • Lloyd, D.K.1    Goodall, D.M.2
  • 12
    • 0030985213 scopus 로고    scopus 로고
    • Determination of enantiomeric excess using a chiral selective separation mode and polarimetric detection
    • Lodevico RG, Bobbit DR, Edkins TJ. Determination of enantiomeric excess using a chiral selective separation mode and polarimetric detection. Talanta 1997;44:1353-1363.
    • (1997) Talanta , vol.44 , pp. 1353-1363
    • Lodevico, R.G.1    Bobbit, D.R.2    Edkins, T.J.3
  • 13
    • 0030944546 scopus 로고    scopus 로고
    • On-line HPLC-exciton CD analysis using a chiral benzoyl agent, (S)-TBMB carboxylic acid: A promising approach toward selective identification of enantiomeric diols and diamines
    • Nishida Y, Kim JH, Ohrui H, Meguro H. On-line HPLC-exciton CD analysis using a chiral benzoyl agent, (S)-TBMB carboxylic acid: a promising approach toward selective identification of enantiomeric diols and diamines. J Am Chem Soc 1997;119:1484-1485.
    • (1997) J Am Chem Soc , vol.119 , pp. 1484-1485
    • Nishida, Y.1    Kim, J.H.2    Ohrui, H.3    Meguro, H.4
  • 14
    • 0024969348 scopus 로고
    • Analytical applications of polarimetry, optical rotatory dispersion and circular dichroism
    • Purdie N, Swallows KA. Analytical applications of polarimetry, optical rotatory dispersion and circular dichroism. Anal Chem 1989;61:77A-89A
    • (1989) Anal Chem , vol.61
    • Purdie, N.1    Swallows, K.A.2
  • 15
    • 0025688088 scopus 로고
    • Circular dichroism detection in high-performance liquid chromatography: Evaluation of the anisotropy factor
    • Bertucci C, Domenici E, Salvation P. Circular dichroism detection in high-performance liquid chromatography: evaluation of the anisotropy factor. J Pharm Biomed Anal 1990;8:843-846.
    • (1990) J Pharm Biomed Anal , vol.8 , pp. 843-846
    • Bertucci, C.1    Domenici, E.2    Salvation, P.3
  • 16
    • 0026540926 scopus 로고
    • Investigation of a circular dichroism spectrophotometer as a liquid chromatography detector for enantiomers: Sensitivity, advantages and limitations
    • Zukowsky J, Tang Y, Berthod A, Armstrong D. Investigation of a circular dichroism spectrophotometer as a liquid chromatography detector for enantiomers: sensitivity, advantages and limitations. Anal Chim Acta 1992;258:83-92.
    • (1992) Anal Chim Acta , vol.258 , pp. 83-92
    • Zukowsky, J.1    Tang, Y.2    Berthod, A.3    Armstrong, D.4
  • 17
    • 0028502996 scopus 로고
    • Chiral detection in high-performance liquid chromatography by vibrational circular dichroism
    • Tran CD, Grishko VI, Huang G. Chiral detection in high-performance liquid chromatography by vibrational circular dichroism. Anal Chem 1994;66:2630-2635.
    • (1994) Anal Chem , vol.66 , pp. 2630-2635
    • Tran, C.D.1    Grishko, V.I.2    Huang, G.3
  • 18
    • 33845378401 scopus 로고
    • Laser-based circular dichroism detector for conventional and microbore liquid chromatography
    • Synovec RE, Yeung ES. Laser-based circular dichroism detector for conventional and microbore liquid chromatography. Anal Chem 1985; 57:2606-2610.
    • (1985) Anal Chem , vol.57 , pp. 2606-2610
    • Synovec, R.E.1    Yeung, E.S.2
  • 19
    • 0025708770 scopus 로고
    • Thermal lens-circular dichroism detector for high performance liquid chromatography
    • Xu M, Tran CD. Thermal lens-circular dichroism detector for high performance liquid chromatography. Anal Chem 1990;62:2467-2471.
    • (1990) Anal Chem , vol.62 , pp. 2467-2471
    • Xu, M.1    Tran, C.D.2
  • 20
    • 0027692924 scopus 로고
    • Sensitive circular dichroism spectroscopy based on nonlinear degenerate four-wave mixing
    • Nunes JA, Tong WG. Sensitive circular dichroism spectroscopy based on nonlinear degenerate four-wave mixing. Anal Chem 1993;65:2990-2994.
    • (1993) Anal Chem , vol.65 , pp. 2990-2994
    • Nunes, J.A.1    Tong, W.G.2
  • 21
    • 0028538685 scopus 로고
    • Universal spectropolarimeter based on overtone circular dichroism measurements in the near-infrared region
    • Tran CD, Grishko VI. Universal spectropolarimeter based on overtone circular dichroism measurements in the near-infrared region. Anal Chem 1994;66:3639-3643.
    • (1994) Anal Chem , vol.66 , pp. 3639-3643
    • Tran, C.D.1    Grishko, V.I.2
  • 22
    • 0032253471 scopus 로고    scopus 로고
    • Vibrational circular dichroism: An incisive tool for stereochemical applications
    • Nafie LA Freedman TB. Vibrational circular dichroism: an incisive tool for stereochemical applications. Enantiomer 1998;3:283-297.
    • (1998) Enantiomer , vol.3 , pp. 283-297
    • Nafie, L.A.1    Freedman, T.B.2
  • 23
    • 0028289907 scopus 로고
    • Analytical determination of enantiomeric purity using Raman optical activity
    • Spencer KM, Edmonds RB, Rauh AD, Carrabba MM. Analytical determination of enantiomeric purity using Raman optical activity. Anal Chem 1994;66:1269-1273.
    • (1994) Anal Chem , vol.66 , pp. 1269-1273
    • Spencer, K.M.1    Edmonds, R.B.2    Rauh, A.D.3    Carrabba, M.M.4
  • 24
    • 0024360835 scopus 로고
    • A review of the application of chiroptical methods to analytical chemistry
    • Gergely AA. A review of the application of chiroptical methods to analytical chemistry. J Pharm Biomed Anal 1989;7:523-541.
    • (1989) J Pharm Biomed Anal , vol.7 , pp. 523-541
    • Gergely, A.A.1
  • 25
    • 0025369099 scopus 로고
    • HPLC resolution of racemic 1,4-Benzodiazepin-2-ones by means of a β-cyclodextrin silica bonded chiral stationary phase
    • Bertucci C, Domenici E, Uccello Barretta G, Salvadori P. HPLC resolution of racemic 1,4-Benzodiazepin-2-ones by means of a β-cyclodextrin silica bonded chiral stationary phase. J Chromatogr 1990;506:617-625.
    • (1990) J Chromatogr , vol.506 , pp. 617-625
    • Bertucci, C.1    Domenici, E.2    Uccello Barretta, G.3    Salvadori, P.4
  • 27
    • 0342282458 scopus 로고    scopus 로고
    • note
    • max) × 100]. Actually, the Chromatographic analysis on chiral stationary phase gives the enantiomeric composition and then the enantiomeric excess.
  • 28
    • 0039851414 scopus 로고
    • Optical rotatory dispersion and absolute configuration of flavanones, 3-hydroxyflavanones and their glycosides
    • Gaffield W, Waiss AC. Optical rotatory dispersion and absolute configuration of flavanones, 3-hydroxyflavanones and their glycosides. JCS Chem Commun 1968:29-31.
    • (1968) JCS Chem Commun , pp. 29-31
    • Gaffield, W.1    Waiss, A.C.2
  • 29
    • 49849107557 scopus 로고
    • Optical rotatory dispersion and absolute configuration of flavanones, 3-hydroxyflavanones and their glycosides. Determination of aglycone chiraliry in flavanone glycosides
    • Gaffield W. Optical rotatory dispersion and absolute configuration of flavanones, 3-hydroxyflavanones and their glycosides. Determination of aglycone chiraliry in flavanone glycosides. Tetrahedron 1970;26: 4093-4108.
    • (1970) Tetrahedron , vol.26 , pp. 4093-4108
    • Gaffield, W.1
  • 30
    • 0028919044 scopus 로고
    • Direct enantiomeric separation of flavanones by high performance liquid chromatography using various chiral stationary phases
    • Ficarra P, Ficarra R, Bertucci C, Tommasini S, Calabrò ML, Costantino D, Carulli M. Direct enantiomeric separation of flavanones by high performance liquid chromatography using various chiral stationary phases. Planta Med 1995;61:171-176.
    • (1995) Planta Med , vol.61 , pp. 171-176
    • Ficarra, P.1    Ficarra, R.2    Bertucci, C.3    Tommasini, S.4    Calabrò, M.L.5    Costantino, D.6    Carulli, M.7
  • 31
    • 0028280906 scopus 로고
    • Determination of optical purity by high-performance liquid chromatography upon nonchiral stationary phases with dual circular dichroism/absorption detection
    • Bertucci C, Salvadori P, Lopes Guimaraes LF. Determination of optical purity by high-performance liquid chromatography upon nonchiral stationary phases with dual circular dichroism/absorption detection. J Chromatogr A 1994;666:535-539.
    • (1994) J Chromatogr A , vol.666 , pp. 535-539
    • Bertucci, C.1    Salvadori, P.2    Lopes Guimaraes, L.F.3
  • 32
    • 37049076115 scopus 로고
    • Synthesis, circular dichroism and absolute stereochemistry of chiral spiroaromatic compounds: 9,9′-spirobifluorene derivatives
    • Harada N, Ono H, Nishiwaki T. Uda H. Synthesis, circular dichroism and absolute stereochemistry of chiral spiroaromatic compounds: 9,9′-spirobifluorene derivatives. JCS Chem Commun 1991:1753-1755.
    • (1991) JCS Chem Commun , pp. 1753-1755
    • Harada, N.1    Ono, H.2    Nishiwaki, T.3    Uda, H.4
  • 33
    • 0000851660 scopus 로고
    • Circular dichroic power due to chiral exciton coupling between two polyacene chromophores
    • Harada N, Takuma Y, Uda H. Circular dichroic power due to chiral exciton coupling between two polyacene chromophores. J Am Chem Soc 1978;100:4029-4036.
    • (1978) J Am Chem Soc , vol.100 , pp. 4029-4036
    • Harada, N.1    Takuma, Y.2    Uda, H.3
  • 34
    • 0029999237 scopus 로고    scopus 로고
    • Structural studies by exciton coupled circular dichroism over a large distance: Porphyrin derivatives of steroids, dimeric steroids and brevetoxin B
    • Matile S, Berova N, Nakanishi K, Fleischhauer J, Woody RW. Structural studies by exciton coupled circular dichroism over a large distance: porphyrin derivatives of steroids, dimeric steroids and brevetoxin B. J Am Chem Soc 1996;118:5198-5205.
    • (1996) J Am Chem Soc , vol.118 , pp. 5198-5205
    • Matile, S.1    Berova, N.2    Nakanishi, K.3    Fleischhauer, J.4    Woody, R.W.5


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