-
1
-
-
0001485034
-
-
Potts, K. E., Editor; Pergamon Press, New York, New York
-
a. Lang, Jr., S. A.; Lin, Y.-I. in "Comprehensive Heterocyclic Chemistry", Potts, K. E., Editor; Vol. 6, Part 4B, Pergamon Press, New York, New York, 1984, pp 61-82.
-
(1984)
Comprehensive Heterocyclic Chemistry
, vol.6
, Issue.PART 4B
, pp. 61-82
-
-
Lang S.A., Jr.1
Lin, Y.-I.2
-
2
-
-
0003540629
-
-
R. H. Wiley, Editor, Interscience Publishers, New York, New York, Several recent synthesis reports
-
b. Quilico, A. in "The Chemistry of Heterocyclic Compounds", R. H. Wiley, Editor, Interscience Publishers, New York, New York, 1962, pp 5-35. Several recent synthesis reports:
-
(1962)
The Chemistry of Heterocyclic Compounds
, pp. 5-35
-
-
Quilico, A.1
-
3
-
-
0000500280
-
-
c. Alberola, A., Banez, J. M., Calvo, L., Rodriguez Rodriguez, M. T., and Sanudo, M. C., J. Heterocycl. Chem., 1993, 30, 467.
-
(1993)
J. Heterocycl. Chem.
, vol.30
, pp. 467
-
-
Alberola, A.1
Banez, J.M.2
Calvo, L.3
Rodriguez Rodriguez, M.T.4
Sanudo, M.C.5
-
4
-
-
0026619782
-
-
d. Wei, X., Fang, J., Hu, Y., Hu, H., Synthesis, 1992, 1205.
-
(1992)
Synthesis
, pp. 1205
-
-
Wei, X.1
Fang, J.2
Hu, Y.3
Hu, H.4
-
5
-
-
0001291073
-
-
e. Moriya, O., Nakamura, H., Kageyama, T., and Urata, Y., Tetrahedron Lett., 1989, 30, 3987.
-
(1989)
Tetrahedron Lett.
, vol.30
, pp. 3987
-
-
Moriya, O.1
Nakamura, H.2
Kageyama, T.3
Urata, Y.4
-
6
-
-
0343581483
-
-
f. Balasundaram, B., Perumal, P. T., Synthetic Communications, 1990, 20, 3161.
-
(1990)
Synthetic Communications
, vol.20
, pp. 3161
-
-
Balasundaram, B.1
Perumal, P.T.2
-
7
-
-
0343581484
-
-
See ref. 1a., pp 114-127
-
a. See ref. 1a., pp 114-127.
-
-
-
-
8
-
-
0001656373
-
-
b. Wunch, K. H., and Boulton, A. J., Adv. Heterocycl. Chem., 1967, 8, 277.
-
(1967)
Adv. Heterocycl. Chem.
, vol.8
, pp. 277
-
-
Wunch, K.H.1
Boulton, A.J.2
-
9
-
-
0011300125
-
-
a. Ogata, M., Matsumoto, H., and Kano, H., Tetrahedron, 1969, 52, 5205.
-
(1969)
Tetrahedron
, vol.52
, pp. 5205
-
-
Ogata, M.1
Matsumoto, H.2
Kano, H.3
-
12
-
-
1942464098
-
-
d. Davis, R. B., and Pizzini, L. C., J. Org. Chem. 1960, 25, 1884.
-
(1960)
J. Org. Chem.
, vol.25
, pp. 1884
-
-
Davis, R.B.1
Pizzini, L.C.2
-
13
-
-
0010924783
-
-
a. Johnson, W. S., and Shelberg, W. E., J. Am. Chem. Soc., 1945, 67, 1745.
-
(1945)
J. Am. Chem. Soc.
, vol.67
, pp. 1745
-
-
Johnson, W.S.1
Shelberg, W.E.2
-
14
-
-
0342711454
-
-
Japan Kokkai JP 48099161
-
b. Suzuka, Y., and Minami, N., Japan Kokkai JP 48099161: Chem. Abstr., 1974, 80:95923.
-
(1974)
Chem. Abstr.
, vol.80
, pp. 95923
-
-
Suzuka, Y.1
Minami, N.2
-
15
-
-
0043137879
-
-
c. Sami, M. I., Gandhi, K. K., and Ray, J. K., Org. Prep. Proced. Int., 1991, 23, 186.
-
(1991)
Org. Prep. Proced. Int.
, vol.23
, pp. 186
-
-
Sami, M.I.1
Gandhi, K.K.2
Ray, J.K.3
-
16
-
-
0028019127
-
-
d. Nitz, T. J., Volkots, D. L., and Aldous, J. A., and Oglesby, R. C., J. Org. Chem., 1994, 59, 5828.
-
(1994)
J. Org. Chem.
, vol.59
, pp. 5828
-
-
Nitz, T.J.1
Volkots, D.L.2
Aldous, J.A.3
Oglesby, R.C.4
-
17
-
-
0000486151
-
-
e. Barber, G. N., and Olofson R. A., J. Org. Chem., 1978, 43, 3015.
-
(1978)
J. Org. Chem.
, vol.43
, pp. 3015
-
-
Barber, G.N.1
Olofson, R.A.2
-
19
-
-
37049080959
-
-
b. Moriya, O., Takenaka, H., Iyoda, M., Urata, Y., and Endo, T., J. Chem. Soc., Perkin Trans 1, 1999, 413.
-
(1999)
J. Chem. Soc., Perkin Trans
, vol.1
, pp. 413
-
-
Moriya, O.1
Takenaka, H.2
Iyoda, M.3
Urata, Y.4
Endo, T.5
-
20
-
-
0027204831
-
-
Sakamoto, T., Uchiyama, D., Kondo, Y., Yamanaka, H., Chem. Pharm. Bull., 1993, 41, 478.
-
(1993)
Chem. Pharm. Bull.
, vol.41
, pp. 478
-
-
Sakamoto, T.1
Uchiyama, D.2
Kondo, Y.3
Yamanaka, H.4
-
21
-
-
0001424311
-
-
a. Beam, C. F., Dyer, M. C. D., Schwarz, R. A., and Hauser, C. R., J. Org. Chem., 1970, 35, 1806.
-
(1970)
J. Org. Chem.
, vol.35
, pp. 1806
-
-
Beam, C.F.1
Dyer, M.C.D.2
Schwarz, R.A.3
Hauser, C.R.4
-
22
-
-
84980213404
-
-
b. Beam, C. F., Foote, R. S., and Hauser, C. R., J. Heterocycl. Chem., 1972, 9, 183.
-
(1972)
J. Heterocycl. Chem.
, vol.9
, pp. 183
-
-
Beam, C.F.1
Foote, R.S.2
Hauser, C.R.3
-
23
-
-
84980250878
-
-
c. Sandifer, R. M., Dasher, L. W., Hollinger, W. M., Thomas, C. W., Reames, D. C., Beam, C. F., Foote, R. S. and Hauser, C. R., J. Heterocycl. Chem., 1975, 12, 1159.
-
(1975)
J. Heterocycl. Chem.
, vol.12
, pp. 1159
-
-
Sandifer, R.M.1
Dasher, L.W.2
Hollinger, W.M.3
Thomas, C.W.4
Reames, D.C.5
Beam, C.F.6
Foote, R.S.7
Hauser, C.R.8
-
24
-
-
0010988010
-
-
d. Perkins, M., Beam, C. F., Dyer, M. C. D., and Hauser, C. R., Org. Synth., 1975, 55, 39.
-
(1975)
Org. Synth.
, vol.55
, pp. 39
-
-
Perkins, M.1
Beam, C.F.2
Dyer, M.C.D.3
Hauser, C.R.4
-
25
-
-
84980256280
-
-
e. Sandifer, R. M., Shaffer, L. M., Hollinger, W. M., Reames, D. C., and Beam, C. F., J. Heterocycl. Chem., 1976, 13, 607.
-
(1976)
J. Heterocycl. Chem.
, vol.13
, pp. 607
-
-
Sandifer, R.M.1
Shaffer, L.M.2
Hollinger, W.M.3
Reames, D.C.4
Beam, C.F.5
-
26
-
-
0017192635
-
-
f. Beam, C. F., Shealy, K. D., Harris, C. E., Shealy, N. L., Dasher, L. W., Hollinger, W. M., Sandifer, R. M., and Reames, D. C., J. Pharm. Sci., 1976, 65, 1408.
-
(1976)
J. Pharm. Sci.
, vol.65
, pp. 1408
-
-
Beam, C.F.1
Shealy, K.D.2
Harris, C.E.3
Shealy, N.L.4
Dasher, L.W.5
Hollinger, W.M.6
Sandifer, R.M.7
Reames, D.C.8
-
27
-
-
84983372540
-
-
a. Fulmer, T. D., Dasher, L. P., Bobb, B. L., Wilson, J. D., Sides, K. L., and Beam, C. F., J. Heterocycl. Chem., 1980, 17, 799.
-
(1980)
J. Heterocycl. Chem.
, vol.17
, pp. 799
-
-
Fulmer, T.D.1
Dasher, L.P.2
Bobb, B.L.3
Wilson, J.D.4
Sides, K.L.5
Beam, C.F.6
-
28
-
-
84985219471
-
-
b. Livingston, M. J., Chick, M. F., Shealy, E. O., Park, D. J., Fulmer, T. D., and Beam, C. F., J. Heterocycl. Chem., 1982, 19, 215.
-
(1982)
J. Heterocycl. Chem.
, vol.19
, pp. 215
-
-
Livingston, M.J.1
Chick, M.F.2
Shealy, E.O.3
Park, D.J.4
Fulmer, T.D.5
Beam, C.F.6
-
29
-
-
84986506358
-
-
c. Huff, A. M., Hall, H. L., Smith, M. J., O'Grady, S. A., Waters, F. C., Fengl, R. W., Welch, J. A., and Beam, C. F., J. Heterocycl. Chem., 1985, 22, 501.
-
(1985)
J. Heterocycl. Chem.
, vol.22
, pp. 501
-
-
Huff, A.M.1
Hall, H.L.2
Smith, M.J.3
O'Grady, S.A.4
Waters, F.C.5
Fengl, R.W.6
Welch, J.A.7
Beam, C.F.8
-
30
-
-
0031569698
-
-
d. Davis, S. E., Church, A. C., Scott, A. S., Throckmorton, H. L., Studer-Martinez, S. L., and Beam, C. F., J. Organometal. Chem., 1997, 533, 125.
-
(1997)
J. Organometal. Chem.
, vol.533
, pp. 125
-
-
Davis, S.E.1
Church, A.C.2
Scott, A.S.3
Throckmorton, H.L.4
Studer-Martinez, S.L.5
Beam, C.F.6
-
31
-
-
0032960865
-
-
e. Williams, A. R., Angel, A. J., French, K. L., Hurst, D. R., Beckman, D. D., and Beam, C. F., Synthetic Communications, 1999, 29, 1977.
-
(1999)
Synthetic Communications
, vol.29
, pp. 1977
-
-
Williams, A.R.1
Angel, A.J.2
French, K.L.3
Hurst, D.R.4
Beckman, D.D.5
Beam, C.F.6
-
32
-
-
0342276312
-
-
f. Williams, A. R., Finefrock, A. E., Townsend, J. D., Angel, A. J., Hurst, D. R., Rampey, M. E., Halkyard, C. E., Studer-Martinez, S. L., and Beam, C. F., The Chemist, 1998, 75, 7.
-
(1998)
The Chemist
, vol.75
, pp. 7
-
-
Williams, A.R.1
Finefrock, A.E.2
Townsend, J.D.3
Angel, A.J.4
Hurst, D.R.5
Rampey, M.E.6
Halkyard, C.E.7
Studer-Martinez, S.L.8
Beam, C.F.9
-
33
-
-
0010995483
-
-
a. Hoskin, D. H. and Olofson, R. A., J. Org. Chem., 1982, 47, 5222.
-
(1982)
J. Org. Chem.
, vol.47
, pp. 5222
-
-
Hoskin, D.H.1
Olofson, R.A.2
-
34
-
-
84986432161
-
-
b. Fos, E., Borras, L., Gasull, M., Mauleon, D., and Carganico, G., J. Heterocycl. Chem. 1992, 29, 203.
-
(1992)
J. Heterocycl. Chem.
, vol.29
, pp. 203
-
-
Fos, E.1
Borras, L.2
Gasull, M.3
Mauleon, D.4
Carganico, G.5
-
35
-
-
0003824559
-
-
John Wiley and Sons, Inc., New York, New York
-
The preparation of the oxime from 1-tetralone involved a minor modification of a well documented procedure where 20 g of hydroxylamine hydrochloride was dissolved in 120 mL of water followed by the addition of 80 mL of 10% NaOH solution. The solution was placed in a flask or beaker and heated on a stir plate while 20 g of 1-tetralone dissolved in 30-40 mL of ethanol was added along with enough extra ethanol to affect the solution. The solution was heated just enough to slowly boil off solvents [fume hood], and finally an oily layer/phase appeared. The mixture was refrigerated, and crystallization occurred immediately. After filtration, the solid was recrystallized from ethanol, and it was dry enough after filtration for immediate use [15-20 min.], although use of a vacuum desiccator is recommended, [80-90 % yield after recrystallization from ethanol]. See also: Shriner, R. L., Hermann, C. K. F., Morrill, T. C., Curtin, D. Y., and Fuson, R. C., "The Systematic Identification of Organic Compounds", seventh edition, John Wiley and Sons, Inc., New York, New York, 1997, p. 323.
-
(1997)
"The Systematic Identification of Organic Compounds", Seventh Edition
, pp. 323
-
-
Shriner, R.L.1
Hermann, C.K.F.2
Morrill, T.C.3
Curtin, D.Y.4
Fuson, R.C.5
-
36
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0343581480
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note
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a. Melting points were obtained with a Mel-Temp II melting point apparatus in open capillary tubes and are uncorrected.
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37
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0343581479
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note
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b. Combustion analyses for C, H and
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