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85153216400
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note
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The torsional angle between opposite triple bonds is defined as follows: C(sp)-center-of-triple-bond-center-of-opposite-triple-bond-C(sp).
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25
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0005403595
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29
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85153326933
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note
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Observed isotopic pattern fits the calculated one.
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30
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85153237506
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Bruker Analytical X-ray Division, Madison, WI
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Bruker Analytical X-ray Division, Madison, WI, 1996.
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31
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85153327311
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Bruker Analytical X-ray System, Madison, WI
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G. M. Sheldrick, Bruker Analytical X-ray System, Madison, WI, 1997.
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