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Volumn 12, Issue 8, 2000, Pages 2065-2067

Three-dimensional open-framework nickel aluminophosphate [NiAlP2O8][C2N2H9]: Assembly of one-dimensional AlP2O83- chains through [NiO5N] octahedra

Author keywords

[No Author keywords available]

Indexed keywords

ALUMINUM PHOSPHATE; ETHYLENE GLYCOL; ETHYLENEDIAMINE; NICKEL; OXYGEN;

EID: 0033802967     PISSN: 08974756     EISSN: None     Source Type: Journal    
DOI: 10.1021/cm000209b     Document Type: Article
Times cited : (22)

References (27)
  • 24
    • 1642636419 scopus 로고    scopus 로고
    • note
    • 4:en:EG. The reaction mixture was further stirred for 1-2 h until it was homogeneous and then was sealed in a Teflon-lined stainless autoclave and heated at 180°C for 20 days under autogenous pressure. The resulting product containing large light green single crystals was filtered, washed thoroughly with deionized water, and dried at ambient temperature.
  • 25
    • 1642605364 scopus 로고    scopus 로고
    • note
    • 2 = 0.0746. Data/restraints/parameters = 1259/0/181. A suitable single crystal was selected for single-crystal X-ray diffraction analysis. Structural analysis was performed on a Siemens SMART CCD diffractometer using graphite-monochromated Mo Kα radiation (λ(Mo Kα)) = 0.71073 Å). The data were collected at a temperature of 20 ± 2°C. Date processing was accomplished with the SAINT processing program (SMART and SAINT (software packages), Siemens Analytical X-ray Instruments, Inc., Madison, WI, 1996). Direct methods were used to solve the structure using the SHELXTL crystallographic software package (SHELXL, version 5.1, Siemens Industral Automation, Inc., 1997). Hydrogen atoms were located by a difference Fourier map and were added to the structure factor calculation. All non-hydrogen atoms were refined anisotropically.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.