Determination of trace amounts of fatty acids in edible oils by capillary gas-liquid chromatography

JAOCS, Journal of the American Oil Chemists' Society

Volumn 77, Issue 6, 2000, Pages 653-657

  Buchgraber, M ^a   Ulberth, F ^a,b   Anklam, E ^a  

^a JOINT RESEARCH CENTRE   (Italy)

^b UNIVERSITY OF NATURAL RESOURCES AND LIFE SCIENCES   (Austria)

Author keywords

[No Author keywords available]

Indexed keywords

ESTERS; FATTY ACIDS; GAS CHROMATOGRAPHY; IONIZATION; LIQUID CHROMATOGRAPHY; SILICA;

FLAME IONIZATION;

OILS AND FATS;

EID: 0033723094     PISSN: 0003021X     EISSN: None     Source Type: Journal    
DOI: 10.1007/s11746-000-0105-6     Document Type: Article

References (10)

1. Official Methods and Recommended Practices of the American Oil Chemists' Society, Fatty Acid Composition by GLC, cis, cis and trans Isomers, American Oil Chemists' Society, Champaign, 1992, AOCS Official Method Ce 1c-89.
2. Official Methods of Analysis of AOAC International, Methyl Esters of Fatty Acids in Oils and Fats, Gas Chromatographic Method, 16th edn., AOAC International, Arlington, 1995, AOAC Official Method 963.22.
3. Standard Methods for the Analysis of Oils, Fats and Derivatives, Gas-Liquid Chromatography of Fatty Acid Methyl Esters, 7th edn., International Union of Pure and Applied Chemistry, Oxford, 1987, Method 2.302.
4. Christie, W.W., Preparation of Ester Derivatives of Fatty Acids for Chromatographic Analysis, in Advances in Lipid Methodology - Two, The Oily Press, Dundee, 1993, pp. 69-111.
5. Commission Regulation (EEC) No. 183/93 of 29 January 1993 Amending Regulation (EEC) No. 2568/91 on the Characteristics of Olive Oil and Olive-Residue Oil and on the Relevant Methods of Analysis, Official Journal L 022, 30/01/1993, pp. 58-68.
6. Mensink, R.P., and P.L. Katan, Lipoprotein Metabolism and Trans Fatty Acids, in Trans Fatty Acids in Human Nutrition, edited by J.L. Sébédio, and W.W. Christie, The Oily Press, Dundee, 1998, pp. 217-234.
7. Ackman, R.G., and T.K. Mag, Trans Fatty Acids and the Potential for Less in Technical Products, in Ibid., pp. 35-58.
8. Grandgirard, A., F. Julliard, J. Prevos, and J.L. Sébédio, Preparation of Geometrical Isomers of Linolenic Acid, J. Am. Oil Chem. Soc. 64:1434-1439 (1987).
9. Bannon, C.D., G.J. Breen, J.D. Craske, N. Tr. Hai, N.L. Harper, and K.L. O'Rourke, Analysis of Fatty Acid Methyl Esters with High Accuracy. III. Literature Review of and Investigation into the Development of Rapid Procedures for the Methoxide-Catalyzed Methanolysis of Fats and Oils, J. Chromatogr. 247:71-89 (1982).
10. Ulberth, F., M. Buchgraber, and A. Boenke, Intercomparison of Methods for the Determination of Trans Fatty Acids in Edible Oils and Fats - Results of the 1st Intercomparison Study, Report EUR 18955 EN, European Commission, Luxembourg, 1999.