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See Supporting Information
-
See Supporting Information.
-
-
-
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42
-
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0345677786
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note
-
(a) When water is used as the solvent, preparation of fresh EDC solution just prior to use is necessary, since carbodiimide reacts slowly with water to form the corresponding urea. (b) Protonated PLL will not form stable adsorbed layers on oxidized PG surfaces; EDC was necessary for binding.
-
-
-
-
43
-
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0345677785
-
-
note
-
During initial scans, films equilibrate with the fluid medium, as evidenced by a significant increase in cell RC (resistance-capacitance) time constant with a constant R, estimated by using the Auto iR Comp function of the BAS-100B/W. While R values varied significantly from film to film (75-140 Ω), a typical example had RC = 1150 ms, R = 108 Ω before scanning, and RC = 1550 ms, R = 108 Ω after one scan. Successive scanning after the first did not change RC or R significantly.
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44
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0000486419
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46
-
-
0345246019
-
-
note
-
Upon addition of EDB to the solution, the peak current increased as the contact time of the coating electrode with the solution increased until it reached a constant value. This may be related to slow permeation of EDB into the film. When the more hydrophilic trichloroacetic acid was used, no such growth of maximum catalytic current was observed.
-
-
-
-
47
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33845373497
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48
-
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0345246021
-
-
note
-
app are under further study.
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