A new convenient procedure to prepare organomanganese reagents from organic halides and activated manganese

Tetrahedron Letters

Volumn 40, Issue 35, 1999, Pages 6407-6410

  Cahiez, Gérard ^a   Martin, Arnaud ^a   Delacroix, Thomas ^a  

^a CNRS   (France)

Author keywords

[No Author keywords available]

Indexed keywords

LITHIUM; MANGANESE; MANGANESE CHLORIDE; MANGANESE DERIVATIVE; ORGANOHALOGEN DERIVATIVE; PYRIDINE DERIVATIVE; REAGENT;

ARTICLE; SYNTHESIS;

EID: 0033609788     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(99)01331-3     Document Type: Article

References (16)

1. For reviews see: (a) Cahiez, G. Butyl Manganese Chloride in Encyclopedia of Reagents for Organic Synthesis, Paquette, L.; Ed., Wiley, Chichester 1995, 2, 925-928.
2. (b) Cahiez, G. Manganese (II) Chloride in Encyclopedia of Reagents for Organic Synthesis, Paquette, L.; Ed., Wiley, Chichester 1995, 5, 3227-3228.
3. (c) Cahiez, G. Anales De QuíMica 1995, 91, 561-578. See also Cahiez, G.; Marquais, S. Pure & Appl. Chem. 1996, 68, 669-679.
4. (c) Cahiez, G. Anales De QuíMica 1995, 91, 561-578. See also Cahiez, G.; Marquais, S. Pure & Appl. Chem. 1996, 68, 669-679.
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11. (a) Kim, S.-H. ; Hanson, M.V. ; Rieke, R.D. Tetrahedron Lett. 1996, 37, 2197-2200.
12. (b) Kim, S.-H. ; Rieke, R.D. Tetrahedron Lett. 1997, 38, 993-996.
13. (c) Rieke, R.D. ; Kim, S.-H. ; Wu, X. J. Org. Chem. 1997, 62, 6921-6927.
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16. 4, filtration and evaporation under vacuo, the product is purified by column chromatography on silica gel (cyclohexane/ethyl acetate 98:2) to give 0.5 g (81%) of 5-dodecanone.