A new and efficient palladium-catalyzed synthesis of a 2,3,4,5- tetrahydro-1H-2,4-benzodiazepine-1,3-dione derivative

Tetrahedron Letters

Volumn 40, Issue 13, 1999, Pages 2623-2624

  Bocelli, Gabriele ^a   Catellani, Marta ^b   Cugini, Federica ^b   Ferraccioli, Raffaella ^c  

^a CSSD   (Italy)

^b 17/A 43100 Parma Italy   (Italy)

^c CSSSSO   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

BENZODIAZEPINE DERIVATIVE; CARBANILAMIDE; CARBON MONOXIDE; ISOINDOLE DERIVATIVE; PALLADIUM; SOLVENT;

ARTICLE; ATMOSPHERIC PRESSURE; CATALYST; CHEMICAL ANALYSIS; CYCLIZATION; ENZYME STABILITY; OXIDATION; PRECURSOR; STEREOCHEMISTRY; SYNTHESIS; X RAY;

EID: 0033605925     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(99)00232-4     Document Type: Article

References (11)

1. For recent examples of syntheses of seven-membered nitrogen compounds see: (a) Tietze L.F.; Schimpf R. Synthesis 1993, 876-880;
2. (b) Grigg R.; Sridharan V. Tetrahedron Lett. 1993, 34, 7471-7474;
3. (c) Wolfe J.P.; Rennels R.A.; Buchwald S.; Tetrahedron 1996, 52, 7525-7546;
4. (d) Bocelli G.; Catellani M.; Chiusoli G.P.; Cugini F., Lasagni B.; Neri Mari M. Inorg. Chim. Acta 1998, 270, 123-129.
5. Weissberger A.; Taylor E.C., Eds. The Chemistry of Heterocyclic Compounds, Vol. 43 (Rosowsky ed), Wiley, New York, 1984.
6. Felix M. A.; Fryer R.I. J. Heterocyclic Chem. 1968, 5, 291-293 and references therein.
7. +, 55), 190 (100).
8. Butula Lj.; Kolbah D.; Butula I. Croat. Chem. Acta 1972, 44, 481-485.
9. 1/C, a = 13.118(3) Å, b = 11.069(3) Å, c = 12.606(2) Å, β = 115.64 (4)°, V = 1650.2(9) Å3. Data were measured on a Siemens AED diffractometer.
10. +), 911(M-I), 910 (M-HI).
11. Brown J.M.; Pèrez-Torrente J.; Alcock N.W.; Clase H.J. Organometallics 1995, 14, 207-213.