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Tetrahedron

Volumn 55, Issue 30, 1999, Pages 9163-9170

A preparation of trifluorolactic aldehyde

(5) Katagiri, Toshimasa a Kutose, Koichi a Shimokawa, Naoya a Kusunoki, Norihiko a Uneyama, Kenji a

a OKAYAMA UNIVERSITY (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

2 BENZOYLOXY 3,3,3 TRIFLUOROPROPANAL; ALDEHYDE; LACTIC ACID DERIVATIVE; PROPIONALDEHYDE; UNCLASSIFIED DRUG;

ARTICLE; HYDROLYSIS; ISOLATION PROCEDURE; OPTICAL RESOLUTION; OXIDATION; PRIORITY JOURNAL; RACEMIC MIXTURE; REACTION ANALYSIS; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 0033597963 PISSN: 00404020 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4020(99)00498-6 Document Type: Article

Times cited : (8)

References (13)

1
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- Konno,T.; Yamazaki, T.; Kitazume,T. Tetrahedron, 1996, 52, 199;
- (1996) Tetrahedron , vol.52 , pp. 199
- Konno, T.¹ Yamazaki, T.² Kitazume, T.³

2
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- Hedhli, A.; Szönyi, S.; Baklouti, A.; Cambon, A. J. Fluorine Chem., 1994, 69, 133.
- (1994) J. Fluorine Chem. , vol.69 , pp. 133
- Hedhli, A.¹ Szönyi, S.² Baklouti, A.³ Cambon, A.⁴

3
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- Bravo, P.; Frigerio, M.; Resnati, G.; J. Org. Chem., 1990, 55, 4216.
- (1990) J. Org. Chem. , vol.55 , pp. 4216
- Bravo, P.¹ Frigerio, M.² Resnati, G.³

4
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- Jpn. Kokai Tokkyo Koho, JP 05-186890
- Kubota, T.; Otake, T.; Katagiri, T. Jpn. Kokai Tokkyo Koho, 1993, JP 05-186890.
- (1993)
- Kubota, T.¹ Otake, T.² Katagiri, T.³

5
- 85069134183
- Jpn. Kokai Tokkyo Koho, JP 07-247266
- Fuchigami, T.; Sano, M.; Katagiri, T. Jpn. Kokai Tokkyo Koho, 1995, JP 07-247266.
- (1995)
- Fuchigami, T.¹ Sano, M.² Katagiri, T.³

6
- 0001591015
- Uneyama, K.; Momota, M.; Hayashida, K.; Itoh, T. J. Org. Chem., 1990, 55, 5364; Uneyama, K.; Momota, M. Tetrahedron Lett., 1989, 30, 2265; Katagiri, T.; Furuhashi, K. Jpn. Kokai Tokkyo Koho, 1993, JP 05-255237.
- (1990) J. Org. Chem. , vol.55 , pp. 5364
- Uneyama, K.¹ Momota, M.² Hayashida, K.³ Itoh, T.⁴

7
- 0000920139
- Uneyama, K.; Momota, M.; Hayashida, K.; Itoh, T. J. Org. Chem., 1990, 55, 5364; Uneyama, K.; Momota, M. Tetrahedron Lett., 1989, 30, 2265; Katagiri, T.; Furuhashi, K. Jpn. Kokai Tokkyo Koho, 1993, JP 05-255237.
- (1989) Tetrahedron Lett. , vol.30 , pp. 2265
- Uneyama, K.¹ Momota, M.²

8
- 0001591015
- Jpn. Kokai Tokkyo Koho, JP 05-255237
- Uneyama, K.; Momota, M.; Hayashida, K.; Itoh, T. J. Org. Chem., 1990, 55, 5364; Uneyama, K.; Momota, M. Tetrahedron Lett., 1989, 30, 2265; Katagiri, T.; Furuhashi, K. Jpn. Kokai Tokkyo Koho, 1993, JP 05-255237.
- (1993)
- Katagiri, T.¹ Furuhashi, K.²

9
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- Hedhli, A.; Baklouti, A.; Cambon, A. Tetrahedron Lett., 1994, 35, 6877.
- (1994) Tetrahedron Lett. , vol.35 , pp. 6877
- Hedhli, A.¹ Baklouti, A.² Cambon, A.³

10
- 85069141980
- 19F NMR
- 19F NMR.

11
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- Katagiri, T.; Obara, F.; Toda, S.; Furuhashi, K. Synlett, 1994, 507-508.
- (1994) Synlett , pp. 507-508
- Katagiri, T.¹ Obara, F.² Toda, S.³ Furuhashi, K.⁴

12
- 85069139821
- 1H NMR, distillation of the reaction mixture gave the aldehyde in 90% yield (0.45 mmol)
- 1H NMR, distillation of the reaction mixture gave the aldehyde in 90% yield (0.45 mmol).

13
- 85069129355
- The optical purity was compared with 2-propyl 2-benzoyloxy-3,3,3-trifluoropropanoate derived from trifluorolactic acid (ref. 8)
- The optical purity was compared with 2-propyl 2-benzoyloxy-3,3,3-trifluoropropanoate derived from trifluorolactic acid (ref. 8).

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