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0344768145
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For related chemistry using nanostructured nickel clusters, see: Reetz, M. T.; Breinbauer, R.; Wedemann, P.; Binger, P. Tetrahedron 1998, 54, 1233.
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22
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0345198688
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note
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2, did not lead to an active catalyst as most of the metal was easily washed off the charcoal.
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23
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0031187658
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Gil, A.; Gandia, L. M.; Montes, M. J. Phys. Chem. Sol. 1997, 58(7), 1079; Gandia, L. M.; Montes, M. J. Catal. 1994, 145, 276-288; Garcia, M. D.; Marales, I. F.; Garzon, F. J. L. Appl. Catal. A 1994, 112, 75.
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43949149398
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Gil, A.; Gandia, L. M.; Montes, M. J. Phys. Chem. Sol. 1997, 58(7), 1079; Gandia, L. M.; Montes, M. J. Catal. 1994, 145, 276-288; Garcia, M. D.; Marales, I. F.; Garzon, F. J. L. Appl. Catal. A 1994, 112, 75.
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Gil, A.; Gandia, L. M.; Montes, M. J. Phys. Chem. Sol. 1997, 58(7), 1079; Gandia, L. M.; Montes, M. J. Catal. 1994, 145, 276-288; Garcia, M. D.; Marales, I. F.; Garzon, F. J. L. Appl. Catal. A 1994, 112, 75.
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Garcia, M.D.1
Marales, I.F.2
Garzon, F.J.L.3
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26
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0344768141
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note
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2O (3 x 100 mL) and distilled THF (2 x 100 mL) and then dried under vacuum (0.5 mmHg) at 100°C with stirring for 12 h. Evaporation of the filtrates led to recovery of 113 mg (0.39 mmol) of Ni(II). Thus, 0.27 g (1.48 mmol) Ni(II) was adsorbed onto 3.75 g of charcoal, leading to 1.48 mmol/ 4.02 g (total weight) or 0.37 mmol Ni(II)/g C.
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0000259867
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Tamao, K.; Sumitani, K.; Kiso, Y.; Zembayashi, M.; Fujioka, A.; Kodama, S.; Nakajima, A.; Kumada, M. Bull. Chem. Soc. Jpn. 1976, 7, 1958; Tamao, K.; Kumada, M. In The Chemistry of the Metal-Carbon Bond; Hartley, F. R., Ed.; John Wiley: New York, 1987; Vol. 4, p 820.
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Fujioka, A.5
Kodama, S.6
Nakajima, A.7
Kumada, M.8
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30
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0001370475
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Hartley, F. R., Ed.; John Wiley: New York
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Tamao, K.; Sumitani, K.; Kiso, Y.; Zembayashi, M.; Fujioka, A.; Kodama, S.; Nakajima, A.; Kumada, M. Bull. Chem. Soc. Jpn. 1976, 7, 1958; Tamao, K.; Kumada, M. In The Chemistry of the Metal-Carbon Bond; Hartley, F. R., Ed.; John Wiley: New York, 1987; Vol. 4, p 820.
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The Chemistry of the Metal-Carbon Bond
, vol.4
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Tamao, K.1
Kumada, M.2
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31
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4244186178
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June 1
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Chem. Eng. News, June 1, 1998, p 24, ibid. July 13, 1998, p 71; see also ibid. December 14, 1998, p 67.
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(1998)
Chem. Eng. News
, pp. 24
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July 13
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Chem. Eng. News, June 1, 1998, p 24, ibid. July 13, 1998, p 71; see also ibid. December 14, 1998, p 67.
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(1998)
Chem. Eng. News
, pp. 71
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33
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December 14
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Chem. Eng. News, June 1, 1998, p 24, ibid. July 13, 1998, p 71; see also ibid. December 14, 1998, p 67.
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(1998)
Chem. Eng. News
, pp. 67
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34
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0345630674
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For an excellent introductory article to the ICP technique, see the following web address: http://mrl.ucsb.edu/mrl/facilities/icp.html.
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35
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0344336114
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Thermo Jarrell Ash Iris HR ICP; 30 s integral time
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Thermo Jarrell Ash Iris HR ICP; 30 s integral time.
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36
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0028337412
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Marck, G.; Villiger, A.; Buchecker, R. Tetrahedron Lett. 1994, 35, 3277.
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(1994)
Tetrahedron Lett.
, vol.35
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Marck, G.1
Villiger, A.2
Buchecker, R.3
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37
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0344768139
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note
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9 containing lithium chloride (85 mg, 2.0 mmol) was then slowly added via cannula. The mixture was warmed to room temperature over 0.5 h, and finally heated to reflux for 12-24 h. The crude reaction mixture was then filtered through a pad of Celite and the filter cake further washed with THF (30 mL). Solvents were then removed on a rotary evaporator, and the resulting oily residue was chromatographed on silica gel.
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