메뉴 건너뛰기




Volumn 40, Issue 43, 1999, Pages 7637-7640

Thraustochytrosides A-C: New glycosphingolipids from a unique marine protist, Thraustochytrium globosum

Author keywords

[No Author keywords available]

Indexed keywords

GLYCOSPHINGOLIPID; THRAUSTOCHYTROSIDE A; THRAUSTOCHYTROSIDE B; THRAUSTOCHYTROSIDE C; UNCLASSIFIED DRUG;

EID: 0033595851     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(99)01562-2     Document Type: Article
Times cited : (33)

References (15)
  • 4
    • 0009772226 scopus 로고    scopus 로고
    • Strain CNK-018 was cultured in a liquid marine medium (B1 medium composed of 2.5 g peptone, 1.5 g yeast extract, 3.0 ml 50% glycerol per 1 L autoclaved filtered seawater) for 3 days while shaking at 150 rpm
    • Strain CNK-018 was cultured in a liquid marine medium (B1 medium composed of 2.5 g peptone, 1.5 g yeast extract, 3.0 ml 50% glycerol per 1 L autoclaved filtered seawater) for 3 days while shaking at 150 rpm.
  • 5
    • 0009775123 scopus 로고    scopus 로고
    • The crude extract was first adsorbed onto Celite and eluted with isooctane, EtOAc and MeOH. The isooctane fraction was further partitioned between hexane and MeOH. The MeOH soluble portion was dried and dissolved in EtOAc before being partitioned with water, to yield a white precipitate. The EtOAc fraction and ppt. were recombined and separated by flash chromatography on a RP C-18 column (30 × 2.5 cm) eluting with 100% MeOH
    • The crude extract was first adsorbed onto Celite and eluted with isooctane, EtOAc and MeOH. The isooctane fraction was further partitioned between hexane and MeOH. The MeOH soluble portion was dried and dissolved in EtOAc before being partitioned with water, to yield a white precipitate. The EtOAc fraction and ppt. were recombined and separated by flash chromatography on a RP C-18 column (30 × 2.5 cm) eluting with 100% MeOH.
  • 6
    • 0009772227 scopus 로고    scopus 로고
    • note
    • 8 · Na, 734.5547; found, 734.5527 (Δ 2.7 ppm).
  • 7
    • 0000363997 scopus 로고
    • Costantino, V.; Fattorusso, E.; Mangoni, A. J. Org. Chem. 1993, 58, 186-191. Sitrin, R. D.; Chan, G.; Dingerdissen, J.; DeBrosse, C.; Mehta, R.; Roberts, G.; Rottschaefer, S.; Stagier, D.; Valenta, J.; Snader, K. M.; Stedman, R. J.; Hoover, J. R. E. J. Antibiot. 1988, 41, 469-480. Costantino, V.; Fattorusso, E.; Mangoni, A.; Di Rosa, M.; Ianaro, A. J. Am. Chem. Soc. 1997, 119, 12465-12470.
    • (1993) J. Org. Chem. , vol.58 , pp. 186-191
    • Costantino, V.1    Fattorusso, E.2    Mangoni, A.3
  • 9
    • 0031585732 scopus 로고    scopus 로고
    • Costantino, V.; Fattorusso, E.; Mangoni, A. J. Org. Chem. 1993, 58, 186-191. Sitrin, R. D.; Chan, G.; Dingerdissen, J.; DeBrosse, C.; Mehta, R.; Roberts, G.; Rottschaefer, S.; Stagier, D.; Valenta, J.; Snader, K. M.; Stedman, R. J.; Hoover, J. R. E. J. Antibiot. 1988, 41, 469-480. Costantino, V.; Fattorusso, E.; Mangoni, A.; Di Rosa, M.; Ianaro, A. J. Am. Chem. Soc. 1997, 119, 12465-12470.
    • (1997) J. Am. Chem. Soc. , vol.119 , pp. 12465-12470
    • Costantino, V.1    Fattorusso, E.2    Mangoni, A.3    Di Rosa, M.4    Ianaro, A.5
  • 12
    • 0009774291 scopus 로고    scopus 로고
    • note
    • 1 H NMR (300 MHz, DMSO): δ 5.02 (H-1″, d, J=3.6), 4.92 (H-2″, dd, J=3.6, 10.1), 5.50 (H-3″, dd, J=10.4, 8.4), 5.02 (H-4″, dd, J=8.4, 11.1), 4.00 (H-5″, m), 4.26 (H-6″, dd, J=4.6, 12.4), 4.12 (H-6″, dd, J=1.81, 12.4).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.