-
2
-
-
0028209483
-
-
Jin, W.; Rinehart, K. L.; Jares-Erijman, E. A. J. Org. Chem. 1994, 59, 144-147.
-
(1994)
J. Org. Chem.
, vol.59
, pp. 144-147
-
-
Jin, W.1
Rinehart, K.L.2
Jares-Erijman, E.A.3
-
3
-
-
0028204397
-
-
Natori, T.; Morita, M.; Akimoto, K.; Koezuka, Y. Tetrahedron 1994, 50, 2771-2784.
-
(1994)
Tetrahedron
, vol.50
, pp. 2771-2784
-
-
Natori, T.1
Morita, M.2
Akimoto, K.3
Koezuka, Y.4
-
4
-
-
0009772226
-
-
Strain CNK-018 was cultured in a liquid marine medium (B1 medium composed of 2.5 g peptone, 1.5 g yeast extract, 3.0 ml 50% glycerol per 1 L autoclaved filtered seawater) for 3 days while shaking at 150 rpm
-
Strain CNK-018 was cultured in a liquid marine medium (B1 medium composed of 2.5 g peptone, 1.5 g yeast extract, 3.0 ml 50% glycerol per 1 L autoclaved filtered seawater) for 3 days while shaking at 150 rpm.
-
-
-
-
5
-
-
0009775123
-
-
The crude extract was first adsorbed onto Celite and eluted with isooctane, EtOAc and MeOH. The isooctane fraction was further partitioned between hexane and MeOH. The MeOH soluble portion was dried and dissolved in EtOAc before being partitioned with water, to yield a white precipitate. The EtOAc fraction and ppt. were recombined and separated by flash chromatography on a RP C-18 column (30 × 2.5 cm) eluting with 100% MeOH
-
The crude extract was first adsorbed onto Celite and eluted with isooctane, EtOAc and MeOH. The isooctane fraction was further partitioned between hexane and MeOH. The MeOH soluble portion was dried and dissolved in EtOAc before being partitioned with water, to yield a white precipitate. The EtOAc fraction and ppt. were recombined and separated by flash chromatography on a RP C-18 column (30 × 2.5 cm) eluting with 100% MeOH.
-
-
-
-
6
-
-
0009772227
-
-
note
-
8 · Na, 734.5547; found, 734.5527 (Δ 2.7 ppm).
-
-
-
-
7
-
-
0000363997
-
-
Costantino, V.; Fattorusso, E.; Mangoni, A. J. Org. Chem. 1993, 58, 186-191. Sitrin, R. D.; Chan, G.; Dingerdissen, J.; DeBrosse, C.; Mehta, R.; Roberts, G.; Rottschaefer, S.; Stagier, D.; Valenta, J.; Snader, K. M.; Stedman, R. J.; Hoover, J. R. E. J. Antibiot. 1988, 41, 469-480. Costantino, V.; Fattorusso, E.; Mangoni, A.; Di Rosa, M.; Ianaro, A. J. Am. Chem. Soc. 1997, 119, 12465-12470.
-
(1993)
J. Org. Chem.
, vol.58
, pp. 186-191
-
-
Costantino, V.1
Fattorusso, E.2
Mangoni, A.3
-
8
-
-
0023929123
-
-
Costantino, V.; Fattorusso, E.; Mangoni, A. J. Org. Chem. 1993, 58, 186-191. Sitrin, R. D.; Chan, G.; Dingerdissen, J.; DeBrosse, C.; Mehta, R.; Roberts, G.; Rottschaefer, S.; Stagier, D.; Valenta, J.; Snader, K. M.; Stedman, R. J.; Hoover, J. R. E. J. Antibiot. 1988, 41, 469-480. Costantino, V.; Fattorusso, E.; Mangoni, A.; Di Rosa, M.; Ianaro, A. J. Am. Chem. Soc. 1997, 119, 12465-12470.
-
(1988)
J. Antibiot.
, vol.41
, pp. 469-480
-
-
Sitrin, R.D.1
Chan, G.2
Dingerdissen, J.3
DeBrosse, C.4
Mehta, R.5
Roberts, G.6
Rottschaefer, S.7
Stagier, D.8
Valenta, J.9
Snader, K.M.10
Stedman, R.J.11
Hoover, J.R.E.12
-
9
-
-
0031585732
-
-
Costantino, V.; Fattorusso, E.; Mangoni, A. J. Org. Chem. 1993, 58, 186-191. Sitrin, R. D.; Chan, G.; Dingerdissen, J.; DeBrosse, C.; Mehta, R.; Roberts, G.; Rottschaefer, S.; Stagier, D.; Valenta, J.; Snader, K. M.; Stedman, R. J.; Hoover, J. R. E. J. Antibiot. 1988, 41, 469-480. Costantino, V.; Fattorusso, E.; Mangoni, A.; Di Rosa, M.; Ianaro, A. J. Am. Chem. Soc. 1997, 119, 12465-12470.
-
(1997)
J. Am. Chem. Soc.
, vol.119
, pp. 12465-12470
-
-
Costantino, V.1
Fattorusso, E.2
Mangoni, A.3
Di Rosa, M.4
Ianaro, A.5
-
12
-
-
0009774291
-
-
note
-
1 H NMR (300 MHz, DMSO): δ 5.02 (H-1″, d, J=3.6), 4.92 (H-2″, dd, J=3.6, 10.1), 5.50 (H-3″, dd, J=10.4, 8.4), 5.02 (H-4″, dd, J=8.4, 11.1), 4.00 (H-5″, m), 4.26 (H-6″, dd, J=4.6, 12.4), 4.12 (H-6″, dd, J=1.81, 12.4).
-
-
-
-
13
-
-
0030186126
-
-
Keusgen, M.; Yu, C. M.; Curtis, J. M.; Brewer, D.; Ayer, S. W. Biochem. Syst. Ecol. 1996, 24, 465-468.
-
(1996)
Biochem. Syst. Ecol.
, vol.24
, pp. 465-468
-
-
Keusgen, M.1
Yu, C.M.2
Curtis, J.M.3
Brewer, D.4
Ayer, S.W.5
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