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gel values as determined by the glass ball method; deviations were observed only for the aromatic solvents.
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56
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0344071797
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A dihedral angle between vicinal hydrogen atoms of 180° corresponds to 100% anti position, see ref 29
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A dihedral angle between vicinal hydrogen atoms of 180° corresponds to 100% anti position, see ref 29.
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0344071793
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note
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d-Spacing for 1 as obtained from the crystal structure, 17.9 Å; for 12 as obtained from a rapidly dried gel in benzene (see also Table 6).
-
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66
-
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0344071792
-
-
The gel in pyridine is only formed at low temperatures <0°C and at concentration > 10% w/v
-
The gel in pyridine is only formed at low temperatures <0°C and at concentration > 10% w/v.
-
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67
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0344071791
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5
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5.
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68
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0000155076
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Crystal structures that have been solved include N-n-octyl-D-gluconamide 1 (see ref 11), N-n-dodecyl-D-gluconamide (see Vollhardt, D.; Gutberlet, T.; Emrich, G.; Fuhrhop, J.-H. Langmuir 1995, 11, 1, 2661), and N-trideca-5,7-diyne-D-gluconamide (see André, C.; Luger, P.; Fuhrhop, J.-H. Carbohydr. Res. 1994, 230, 31).
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0344503046
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Crystal structures that have been solved include N-n-octyl-D- gluconamide 1 (see ref 11), N-n-dodecyl-D-gluconamide (see Vollhardt, D.; Gutberlet, T.; Emrich, G.; Fuhrhop, J.-H. Langmuir 1995, 11, 1, 2661), and N-trideca-5,7-diyne-D-gluconamide (see André, C.; Luger, P.; Fuhrhop, J.-H. Carbohydr. Res. 1994, 230, 31).
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0344933838
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Upon heating, a rearrangement of the molecules in the crystal from head-to-tail to head-to-head occurs
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Upon heating, a rearrangement of the molecules in the crystal from head-to-tail to head-to-head occurs.
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76
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