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note
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2: C, 75.19; H, 10.41; N, 4.38. Found C, 75.08; H, 10.67; N, 4.90.
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22
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84920313016
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A typical procedure for gelation test: a weighed sample was mixed with an organic fluid (2 mL) in a test tube with screw cap (inside diameter; 14 mm) and the mixture was heated until the solid was dissolved. The resulting solution was cooled at 25 °C for 2 h and then the gelation was checked visually. When upon inversion there was no fluid running down the walls of the tube, we judged it "gel". When a highly viscous solution was formed, it was distinguished as "viscous fluid" from the gel. When the samples caused gelation, we quantitatively evaluated the gelation ability by minimum gel concentrations which are the minimum concentrations of gelators necessary for gelation at 25 °C
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10. A typical procedure for gelation test: a weighed sample was mixed with an organic fluid (2 mL) in a test tube with screw cap (inside diameter; 14 mm) and the mixture was heated until the solid was dissolved. The resulting solution was cooled at 25 °C for 2 h and then the gelation was checked visually. When upon inversion there was no fluid running down the walls of the tube, we judged it "gel". When a highly viscous solution was formed, it was distinguished as "viscous fluid" from the gel. When the samples caused gelation, we quantitatively evaluated the gelation ability by minimum gel concentrations which are the minimum concentrations of gelators necessary for gelation at 25 °C.
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23
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33845185315
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