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PCT Int. Appl. WO 9801478 A1 980115
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3. Rizzardo, E.; Chiefari, J.; Chong, Y.K.; Ercole, F.; Krstina, J.; Jeffery, J.; Le, T.P.T.; Mayadunne, R.T.A.; Meijs, G.F.; Moad, C.L.; Moad, G.; Thang, S.H. Macromol. Symp., in press.
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18
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84920309926
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Tetramethylthiuram disulfide was purchased from Aldrich Co. and used as received
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16. Tetramethylthiuram disulfide was purchased from Aldrich Co. and used as received.
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19
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84920309925
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2/KI solution
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2/KI solution.
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20
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0000003942
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18. Fuchigami, T.; Chen, C.S.; Nonaka, T.; Yen, M.Y.; Tien, H.J. Bull. Chem. Soc. Jpn., 1986, 59, 487.
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Fuchigami, T.1
Chen, C.S.2
Nonaka, T.3
Yen, M.Y.4
Tien, H.J.5
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21
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0001575636
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19. To ensure a sufficient number of radical (R·). Typically 30-50% of radicals formed from thermal decomposition of an azo-compound are consumed by self reaction within the solvent cage, see, for example, Moad, G.; Rizzardo, E.; Solomon, D.H.; Johns, S.R.; Willing, R.I. Makromol. Chem., Rapid Commun., 1984, 5, 793.
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Makromol. Chem., Rapid Commun.
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, pp. 793
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Moad, G.1
Rizzardo, E.2
Solomon, D.H.3
Johns, S.R.4
Willing, R.I.5
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25
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84920309924
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All new compounds (1a)-(1g) gave satisfactory spectroscopic data
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22. All new compounds (1a)-(1g) gave satisfactory spectroscopic data.
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