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0001091186
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In principle, the starting homoallylic alcohol a can be made in optically pure form through the now well established asymmetric aldol technology: Moon Kirn, B.; Williams, S. F. and Masamune, S., In: Comprehensive Organic Synthesis, Editors: B. Trost and I. Fleming, Pergamon Press, 1991, Vol. 2, p. 239-275.
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51
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0013628631
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note
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Inverse order of addition leads to the decomposition of S-alkoxycarbonyl xanthate. For the mechanism of this anionic chain reaction see ref. (4a).
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