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33747566101
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The cyclic peptides are synthesized by classical methods of peptide synthesis
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The cyclic peptides are synthesized by classical methods of peptide synthesis.
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17
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33747580684
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Dissertation, Technische Universität München, Germany
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Thiol peptide A with the N-succinylcysteamide anchor is synthesized by reaction of the peptide with succinic anhydride and coupling of S-tritylcysteamine: D. Finsinger, Dissertation, Technische Universität München, Germany, 1997.
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Finsinger, D.1
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The synthesis of the thiol peptide B with the 3-sulfanylpropionic amide anchor is described in the patent of A. Jonczyk, S. Goodman, B. Diefenbach, A. Sutter, H. Kessler (Merck), WO-A 97/14716,1997 [Chem. Abstr. 1997, 127(2), 17965].
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20
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33747552466
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note
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The PMMA surfaces are coated by dissolution of the acrylated peptide in small amounts of DMSO, successive dilution with isopropanol, and radical polymerization with campher quinone. The surfaces thus obtained were washed several times and sterilized by γ irradiation.
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21
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0020609362
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22
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33747532507
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note
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3).
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23
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33747536208
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note
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1H NMR spectroscopy (250 MHz) as well as HPLC-MS. The expected spectra were obtained.
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24
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0002832133
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The cell proliferation of the cells was determined by the WST-1 procedure: J. A. Cook, J. B. Mitchell, J. Immunol. Methods 1983, 65, 55-63.
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