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0013516889
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note
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8. An oil bath with an effecient stirrer was partitioned by wire mesh to ensure a uniform temperature throughout the experiment. The temperature in each section of the oil bath was confirmed to be same. Normal phase HPLC was performed using ethyl acetate : hexane (30 :70) as the eluent. Absorbance was recorded at fixed wave length of 290 nm.
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14
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0013518968
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note
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10. All solvents were HPLC grade and used directly without further purification. In the case of benzene and THF, rates were obtained from both distilled and non-distilled HPLC grade solvents. The half-life difference between distilled and non-distilled solvent was negligible.
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17
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0013516890
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note
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0bs. correlation coefficient = 0.994. See ref. 6.
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19
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0001457942
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