Preparation, characterization, and structural determination of cubic and triclinic tris (tetra-n-butylammonium) hexakisisothiocyanatoscandate (III)

Journal of Molecular Structure

Volumn 479, Issue 1, 1999, Pages 31-39

  Mullica, Donald F ^a   Kautz, Jason A ^a   Farmer, J Matt ^a   Sappenfield, Eric L ^a  

^a BAYLOR UNIVERSITY   (United States)

Author keywords

Centrosymmetric; Dimorphic; IR NMR; Isothiocyanate complexes; X ray structure

Indexed keywords

AMMONIUM DERIVATIVE; ISOTHIOCYANIC ACID DERIVATIVE;

ARTICLE; CRYSTAL STRUCTURE; STRUCTURE ANALYSIS; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 0033551068     PISSN: 00222860     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0022-2860(98)00811-4     Document Type: Article

References (26)

1. Sarkar P.B. Ann. Chim. [X]. 8:1927;207.
2. Urbain G., Sarkar P.B. C.R. Aca. Sci. Paris. 185:1927;593.
3. Sas T.M., Gagarina V.A., Komissarova L.N., Gulia V.G. Zh. Neorg. Khim. 15:1970;1255.
4. Eremin Y.G., Katochkina V.S., Komissarova L.N. Zh. Neorg. Khim. 15:1970;2067.
5. Gulia V.G., Komissarova L.N., Krasnoyarskaya A.A., Sas T.M. Zh. Neorg. Khim. 15:1970;966.
6. L.N. Komissarova, Y.G. Eremin, V.S. Katochkina, T.M. Sas, Zh. Neorg. Khim., 16 (1971) 2955 and 3224.
7. Hiltunen L., Hölsä J., Strek W., Jezowska-Trzebiatowska B. Acta Crystallogr. C43:1987;2063.
8. Thompson L.C., Radonovich L.J. Acta Crystallogr. C46:1990;1618.
9. Mullica D.F., Kautz J.A., Sappenfield E.L. Inorg. Chim. Acta. 256:1997;115.
10. Einstein F.W.B., Gilbert M.M., Tuck D.G., Vogel P.L. Acta Crystallogr. B32:1976;2234.
11. D.F. Mullica, J.A. Kautz, E.L. Sappenfield, J. Chem. Crystallogr., (1998) submitted.
12. Li B., Zhang Y., Jin T., Huang C., Xu G., Han Y., Shi N. Acta Scientiarum Naturalium. 31:(4):1995;394.
13. Burmeister J.L., Patterson S.D., Deardorff E.A. Inorg. Chim. Acta. 3:1969;105.
14. J.J. Habeeb, D.G. Tuck, J. Chem. Soc., Dalton Trans., (1973) 96.
15. S.J. Patel, D.B. Sowerby, D.G. Tuck, J. Chem. Soc., (A) (1967) 1187.
16. R.B. Roof, Jr. LASL Rep., Los Alamos Scientific Laboratory (1968).
17. Nelson J.B., Riley D.P. Proc. Phys. Soc. (London). 57:1945;477.
18. Smith G.S., Synder R.L. J. Appl. Crystallogr. 12:1979;60.
19. DeWolff P.M. J. Appl. Crystallogr. 1:1968;108.
20. D.E. Appleman, H.T. Evans, Jr. US Geological Survey, Doc. PB2-16188, U. S. Nat. Tech Info. Serv. (1973).
21. Enraf-Nonius, VAX Structure Determination Package, (1985) Delft, The Netherlands.
22. SHELXTL-PC, Siemens Analytical X-ray Instruments, Madison, WI, USA (1989).
23. Gabe E.J., LePage Y., Charland J.-P., Lee F.L., White P.S. J. Appl. Crystallogr. 22:1989;384.
24. Ibers J.A., Hamilton W.C. International Tables for X-ray Crystallography. 4:1974;Kynoch Press, Birmingham, UK.
25. A.G. Orpen, L. Brammer, O. Kennard, D.G. Watson, R. Taylor, J. Chem. Soc., Dalton Trans., (1989) S1.
26. Pauling L. The Nature of the Chemical Bond. 3 :1960;Cornell University Press, NY. pp. 233 and 257.