The synthesis and structure of mixed subphthalocyanine/subnaphthalocyanine complexes

Tetrahedron Letters

Volumn 40, Issue 46, 1999, Pages 8055-8058

  Stork, Jay R ^a   Potucek, Richard J ^a   Durfee, William S ^a   Noll, Bruce C ^b  

^a BUFFALO STATE COLLEGE   (United States)

^b UNIVERSITY OF COLORADO   (United States)

Author keywords

Boron; Boron compounds; Dyes; Macrocycles; X ray crystal structure

Indexed keywords

BORON; DYE; MACROCYCLIC COMPOUND; NAPHTHALENE DERIVATIVE; PHTHALIC ACID DERIVATIVE; PHTHALOCYANINE DERIVATIVE;

ARTICLE; COMPLEX FORMATION; CRYSTAL STRUCTURE; CYCLIZATION; STRUCTURE ANALYSIS; SYNTHESIS;

EID: 0033550243     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(99)01710-4     Document Type: Article

References (14)

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10. 6: 624.0308). Mass spectra were obtained at the Michigan State University Mass Spectrometry Facility, which is supported in part by a grant (DRR-00480) from the Biotechnology Research Technology Program National Center for Research Resources, National Institute of Health.
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13. 1/2, where M=number of reflections and N=number of parameters refined.
14. Two molecules of 1-methylnapthalene were located in the asymmetric unit. These were grossly disordered and the electron density and void space were analyzed using PLATON and SQUEEZE (Spek, 1998, Univ. Utrecht, Utrecht, The Netherlands). Analysis confirmed the 1-methylnapthalene model. SQUEEZE generated a new Fobs file after subtracting contributions from these regions of disordered electron density. The model fit improved by 50%.