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note
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2 with all non-hydrogen atoms anisotropically defined. For 9735 observed reflections [I > 2σ(I)], 689 parameters, and 99 restraints, the conventional R is 0.0505 (wR2 = 0.1531 for 11634 independent reflections). Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication nos. CCDC-119248 (4) and CCDC-119249 (9). Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: (+44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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