Chalcogenatetrasilacyclopentenes: Five-membered rings with endocyclic Si-Si double bonds

Angewandte Chemie - International Edition

Volumn 38, Issue 13-14, 1999, Pages 2010-2012

  Grybat, Andreas ^a   Boomgaarden, Sven ^a   Saak, Wolfgang ^a   Marsmann, Heinrich ^b   Weidenbruch, Manfred ^a  

^a UNIVERSITY OF OLDENBURG   (Germany)

^b UNIVERSITY OF PADERBORN   (Germany)

Author keywords

Chalcogens; Heterocycles; Multiple bonds; Silicon

Indexed keywords

SILICON DERIVATIVE;

ARTICLE; CRYSTAL STRUCTURE; CRYSTALLIZATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REACTION ANALYSIS; SYNTHESIS;

EID: 0033549502     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1521-3773(19990712)38:13/14<2010::AID-ANIE2010>3.0.CO;2-T     Document Type: Article

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19. max = 52°; of 60004 measured reflections, 17885 were independent and 8548 observed with I > 2σ(I). R1 = 0.0548, wR2 (all data) = 0.0985 for 879 parameters. Crystallogaphic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication nos. CCDC-116 227 (5), CCDC-116 228 (6), and CCDC-116 229 (7) Copies of the data can be obtained free of charge on application to CCDC, 12 Union Raod, Cambridge CB2 1EZ, UK (fax: (+44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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