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note
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Radical cyclization of acrylamide 3d in the presence of titanium tetraisopropoxide leads to identical results than in the absence of the Lewis acid.
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A new set of MM2-parameters introduced by Houk indicate the crucial role of the C(acyl)-C(rad)-C(alkene) torsion angle in related acyl-5-hexenyl radical cyclizations. See Broeker, J. L.; Houk, K. N. J. Org. Ckem. 1991, 56, 3651. For early MM2 calculation on amides, see Schnur, D. M.; Yuh, Y. H.; Dalton, D. R. J. Org. Chem. 1989, 54, 3779.
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A new set of MM2-parameters introduced by Houk indicate the crucial role of the C(acyl)-C(rad)-C(alkene) torsion angle in related acyl- 5-hexenyl radical cyclizations. See Broeker, J. L.; Houk, K. N. J. Org. Ckem. 1991, 56, 3651. For early MM2 calculation on amides, see Schnur, D. M.; Yuh, Y. H.; Dalton, D. R. J. Org. Chem. 1989, 54, 3779.
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44
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0344362894
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note
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* optimization, as implemented in PcSpartan Plus (Wave function Inc., 1997).
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