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For the self-inclusion and dimerization of a deep cavitand having p-methoxycarbonylphenyl groups at the upper rim, see: von dem Bussche-Hünnefeld, C.; Helgeson, R. C.; Bühring, D.; Knobler, C. B.; Cram, D. J. Croat. Chim. Acta 1996, 69, 447.
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85038143100
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note
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w=0.110 using 4113 unique reflections (I>2.0σ(I)). The disordering of the non-hydrogen-bonded DMF caused the rather high R values.
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23
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85038140630
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note
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Recrystallization of 1 from pyridine and p-xylene gave cocrystals composed of 1:p-xylene:pyridine=1:2:4.
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