A simple and effective procedure for removal of tri-n-butyltin halides from reaction mixtures

Tetrahedron Letters

Volumn 40, Issue 37, 1999, Pages 6729-6730

  Edelson, Benjamin S ^a   Stoltz, Brian M ^a   Corey, E J ^a  

^a HARVARD UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

BUTYLTIN DERIVATIVE; CESIUM; FLUORIDE ION; ORGANIC COMPOUND; SILICA GEL;

ARTICLE; CHEMICAL REACTION KINETICS; DEALKYLATION; MOLECULAR INTERACTION; REACTION ANALYSIS; SOLID STATE;

EID: 0033543611     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(99)01394-5     Document Type: Article

References (8)

1. Dictionary of Reagents in Organic Synthesis; Paquette, L. A., Ed.; John Wiley and Sons: New York, 1995; pp. 5016-5023.
2. Smith, P. J. Chemistry of Tin; 2nd Ed.; International Thomson Publishing: London, 1998.
3. Pereyre, M.; Quintard, J.-P.; Rahm, A. Tin in Organic Synthesis; Butterworths: London, 1987.
4. Busch-Petersen, J.; Bo, Y.; Corey, E. J. Tetrahedron Lett. 1999, 40, 2065.
5. For alternative protocols for the removal of tin salts, see: (a) Curran, D. P.; Chang, C.-T. J. Org. Chem. 1989, 54, 3140.
6. (b) Milstein, D.; Stille, J. K. J. Am. Chem. Soc. 1978, 100, 3636.
7. (c) Liebner, J. E.; Jacobus, J. J. Org. Chem. 1979, 44, 449.
8. (d) Crich, D.; Sun, S. J. Org. Chem. 1996, 61, 7200.