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Alkaline hydrolysis of the reaction mixture is necessary to liberate the phosphine.
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Alkaline hydrolysis of the reaction mixture is necessary to liberate the phosphine.
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7
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0344812205
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note
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3-THF concentration of 0.55 M.
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Although all the reactions were completed under reflux, TLC often indicated a significant degree of reduction at room temperature.
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Although all the reactions were completed under reflux, TLC often indicated a significant degree of reduction at room temperature.
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10
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0345243329
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note
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15).
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