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Volumn 121, Issue 48, 1999, Pages 11086-11092

Reductive elimination of α-phosphinozirconocene iminoacyl complexes: First evidence of neutral η1-imine zirconocene. Synthesis of bi- or tricyclic β-phosphino imines

Author keywords

[No Author keywords available]

Indexed keywords

IMINE;

EID: 0033537024     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja990502g     Document Type: Article
Times cited : (35)

References (48)
  • 2
    • 0003565155 scopus 로고
    • Hartley, F. R., Patai, S., Eds.; J. Wiley & Sons: Chichester, Carbon-Carbon Bond Formation Using Organometallic Compounds.
    • The Chemistry of the Metal-Carbon Bond; Hartley, F. R., Patai, S., Eds.; J. Wiley & Sons: Chichester, 1985; Vol. 3 (Carbon-Carbon Bond Formation Using Organometallic Compounds).
    • (1985) The Chemistry of the Metal-Carbon Bond , vol.3
  • 11
    • 0028280351 scopus 로고
    • (b) Davis, J. M.; Whitby, R. J.; Jaxa-Chamiec, A. Tetrahedron Lett. 1994, 35, 1445. A formal reductive elimination/ring contraction reaction has been described from treatment of a 1-zircona-2-azacyclopentene with BuNC and MeOH to form a C-N bond.
    • (1994) Tetrahedron Lett. , vol.35 , pp. 1445
    • Davis, J.M.1    Whitby, R.J.2    Jaxa-Chamiec, A.3
  • 16
    • 84920342154 scopus 로고    scopus 로고
    • 2); see ref 2a
    • 2); see ref 2a.
  • 20
    • 84920352742 scopus 로고    scopus 로고
    • 1H INEPT NMR experiments
    • 1H INEPT NMR experiments.
  • 26
    • 0027658856 scopus 로고
    • and references therein
    • (b) Broene R. D.; Buchwald S. L. Science 1993, 261, 1696 and references therein.
    • (1993) Science , vol.261 , pp. 1696
    • Broene, R.D.1    Buchwald, S.L.2
  • 35
    • 0000276712 scopus 로고
    • Wilkinson, G., Gillard, R. D., McCleverty, J. A., Eds.; Pergamon Press: Oxford, England, Chapters 20.1 and 21.2 and references therein
    • Calligaris, M.; Randaccio, L. In Comprehensive Coordination Chemistry; Wilkinson, G., Gillard, R. D., McCleverty, J. A., Eds.; Pergamon Press: Oxford, England, 1987; Chapters 20.1 and 21.2 and references therein.
    • (1987) Comprehensive Coordination Chemistry
    • Calligaris, M.1    Randaccio, L.2
  • 36
    • 84920359145 scopus 로고    scopus 로고
    • note
    • 2-imine zirconocene structure is reasonable to explain the synthesis of 7a,b, the formation of this intermediate in the preparation of 5b is more questionable, as it has been demonstrated that it is possible to displace a titanium metal center from its unreduced imine group by addition of external ligands, see ref 3c,d.
  • 37
    • 84920352275 scopus 로고    scopus 로고
    • It is of interest to note that addition of HCl on 5b does not give 7b
    • It is of interest to note that addition of HCl on 5b does not give 7b.
  • 47
    • 0004265370 scopus 로고    scopus 로고
    • Chemical Crystallography Laboratory, University of Oxford, Oxford, UK
    • Watkin, D. J.; Prout, C. K.; Pearce, L. J. CAMERON; Chemical Crystallography Laboratory, University of Oxford, Oxford, UK, 1996.
    • (1996) CAMERON
    • Watkin, D.J.1    Prout, C.K.2    Pearce, L.J.3


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.