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39
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0344765670
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note
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13C NMR: δ = 41.8, 41.1.
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40
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0345196143
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note
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3. Crystallographic data (excluding structure factors) for the structure reported in this paper have been deposited with the Cambridge Crystallographic Data Centre as supplementary publication no. CCDC-124679. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 IEZ, UK (fax: (+ 44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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0346669475
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44
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0344333617
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note
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This distance corresponds to the normal spacing between the planes formed by each phenylene ring.
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46
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0345628167
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26144444686
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48
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0344765669
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note
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1.
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49
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0345196142
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note
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o): 11.41 (57.48), 9.54 (92.87), 8.09 (100), 6.84 (71.73), 6.57 (15.97), 5.83 (53.45), 5.81 (44.38), 4.98 (33.54), 4.05 (22.68), 3.90 (16.25), 3.80 (17.24), 3.73 (20.69), 3.69 (33.31), 3.54 (31.58), 3.50 (19.89), 3.29 (28.99), 3.04 (20.70).
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