Colloidal Gold Aerogels: Preparation, Properties, and Characterization

Langmuir

Volumn 15, Issue 3, 1999, Pages 674-680

  Anderson, Michele L ^a   Morris, Catherine A ^a   Stroud, Rhonda M ^a   Merzbacher, Celia I ^a   Rolison, Debra R ^a  

^a NAVAL RESEARCH LABORATORY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CATALYSIS; GAS ADSORPTION; GOLD; NANOSTRUCTURED MATERIALS; NEUTRON SCATTERING; NITROGEN; PARTICLE SIZE ANALYSIS; PORE SIZE; SILICA; SURFACE PHENOMENA; TRANSMISSION ELECTRON MICROSCOPY;

PLASMON RESONANCE; SMALL-ANGLE NEUTRON SCATTERING;

AEROGELS;

EID: 0033514189     PISSN: 07437463     EISSN: None     Source Type: Journal    
DOI: 10.1021/la980784i     Document Type: Article

References (58)

1. Hrubesh, L. W. Chem. Ind. 1990, 824.
2. Hrubesh, L. W.; Poco, J. F. J. Non-Cryst. Solids 1995, 188, 46.
3. Braun, S.; Rappoport, S.; Zusmen, R.; Avnir, D.; Ottolenghi, M. Mater. Lett. 1990, 10, 1.
4. Dave, B. C.; Dunn, B.; Valentine, J. S.; Zink, J. I. Anal. Chem. 1994, 68, 1120A.
5. Badini, G. E.; Grattan, K. T. V.; Tseung, A. C. C. Rev. Sci. Instrum. 1995, 66, 4034.
6. Kuleshov, A. P.; Dmitrieva, G. A. J. Opt. Technol. 1996, 63, 252.
7. Narang, U.; Dunbar, R. A.; Bright, F. V.; Prasad, P. N. Appl. Spectrosc. 1993, 47, 1700.
8. Ingersoll, C. M.; Bright, F. V. CHEMTECH 1997, 27, 26.
9. Kistler, S. S. Nature 1931, 127, 741.
10. Nicolaon, G. A.; Teichner, S. J. Bull. Soc. Chim. Fr. 1968, 1900.
11. Gessler, H. D.; Goswami, P. C. Chem. Rev. 1989, 89, 765.
12. Fricke, J. Sci. Am. 1988, 258, 92.
13. Hüsing, N.; Schubert, U. Angew. Chem., Int. Ed. Engl. 1998, 37, 22.
14. Gacoin, T.; Chaput, F.; Boilot, J.-P. Chem. Mater. 1993, 5, 363.
15. Akbarian, F.; Dunn, B. S.; Zink, J. I. J. Raman Spectrosc. 1996, 27, 775.
16. Kutsch, B.; Lyon, O.; Schmitt, M.; Mennig, M.; Schmidt, H. J. Non-Cryst. Solids 1997, 217, 143.
17. Yazawa, T.; Kadono, K.; Tanaka, H.; Sakaguchi, T.; Tsubota, S.; Kuraoka, K.; Miya, M.; De-Xian, W. J. Non-Cryst. Solids 1994, 170, 105.
18. Gacoin, T.; Chaput, F.; Boilot, J.-P.; Jaskierowicz, G. Chem. Mater. 1993, 5, 1150.
19. Mennig, M.; Schmitt, M.; Becker, U.; Jung, G.; Schmidt, H. SPIE Sol-Gel Optics III 1994, 2288, 130.
20. Wang, J.; Pamidi, P. V. A. Anal. Chem. 1997, 69, 4490.
21. Mizushima, Y.; Hori, M. Appl. Catal. A 1992, 88, 137.
22. Ye, S.; Vijh, A. K.; Wang, Z.-Y.; Dao, L. H. Can. J. Chem. 1997, 75, 1666.
23. Horisberger, M.; Rosset, J. J. Histochem. Cytochem. 1977, 25, 296.
24. Turkevich, J.; Garton, G.; Stevenson, P. C. J. Colloid Sci. Suppl. 1954, 1, 26.
25. Russo, R. E.; Hunt, A. J. J. Non-Cryst. Solids 1986, 86, 219.
26. Merzbacher, C. I.; Barker, J. G.; Swider, K. E.; Rolison, D. R. J, Non-Cryst. Solids 1998, 224, 92.
27. Ellerby, L. M.; Nishida, C. R.; Nishida, F.; Yamanaka, S. A.; Dunn, B.; Valentine, J. I.; Zink, J. I. Science 1992, 225, 1113.
28. Merzbacher, C. I.; Barker, J. G.; Swider, K. E.; Ryan, J. V.; Bernstein, R. A.; Rolison, D. R. J. Non-Cryst. Solids 1998, 225, 234.
29. Morris, C. A.; Anderson, M. L.; Merzbacher, C. I.; Stroud, R. M.; Rolison, D. R. Manuscript in preparation.
30. Mie, G. Ann. Phys. (Leipzig) 1908, 25, 377.
31. Heilweil, E. J.; Hochstrasser, R. M. J. Chem. Phys. 1985, 82, 4762.
32. Wilcoxon, J. P.; Martin, J. E.; Schaefer, D. W. Phys. Rev. A 1989, 39, 2675.
33. Khlebtsov, N. G.; Bogatyrev, V. A.; Dykman, L. A.; Mel'nikov, A. G. Opt. Spectrosc. 1996, 80, 128.
34. Bloemer, M. J.; Haus, J. W.; Ashley, P. R. J. Opt. Soc. Am. B 1990, 7, 790.
35. Liz-Marzán, L. M.; Giersig, M.; Mulvaney, P. Chem. Commun. 1996, 731.
36. Liz-Marzán, L. M.; Giersig, M.; Mulvaney, P. Langmuir 1996, 12, 4329.
37. CRC Handbook of Chemistry and Physics, 77th ed.; Lide, D. R., Ed.; CRC Press: New York, 1996.
38. Schaefer, D. W.; Keefer, K. D. Phys. Rev. Lett. 1986, 56, 2199.
39. Craievich, A.; Aegerter, M. A.; dos Santos, D. I.; Woignier, T.; Zarzycki, J. J. Non-Cryst. Solids 1986, 86, 394.
40. Emmerling, A.; Gross, J.; Gerlach, R.; Goswin, R.; Reichenauer, G.; Fricke, J.; Haubold, H.-G. J. Non-Cryst. Solids 1990, 125, 230.
41. 2 samples, due to the smaller contrast between silica and gold vs silica and air.
42. Merzbacher, C. I.; Barker, J. G.; Swider, K. E.; Rolison, D. R. Adv. Colloid Interface Sci. 1998, 76-77, 57.
43. Webb, P. A.; Orr, C. Analytical Methods in Fine Particle Technology; Micromeritics Instrument Corp.: Norcross, GA, 1997.
44. Schuck, G.; Dietrich, W.; Fricke, J. In Aerogels; Fricke, J., Ed.; Springer-Verlag: Berlin, 1986.
45. Einarsrud, M.-A.; Farbrodt, L. E.; Haereid, S. In Chemical Processing of Advanced Materials; Hench, L. I., West, J. K., Eds.; John Wiley: New York, 1992.
46. Brinker, C. J.; Scherer, G. W. Sol-Gel Science; Academic Press: New York, 1990.
47. Fricke, J.; Emmerling, A. In Chemical Processing of Advanced Materials; Hench, L. L., West, J. K., Eds.; John Wiley: New York, 1992; pp 3-17.
48. This result is distinctly different from the case in which a preformed silica gel soaked in Au sol visibly takes up Au colloid but the "absorbed" colloid visibly flushes out of the gel by washing.
49. Swider, K. E.; Rolison, D. R. Unpublished results, 1996.
50. Nuzzo, R. G.; Zegarski, B. R.; Dubois, L. H. J. Am. Chem. Soc. 1987, 109, 733.
51. Morris, C. A.; Rolison, D. R. Unpublished results, 1997.
52. Brust, M.; Walker, M.; Bethell, D.; Schiffrin, D. J.; Whyman, R. J. Chem. Soc., Chem. Commun. 1994, 801.
53. Grabar, K. C.; Freeman, R. G.; Hommer, M. B.; Natan, M. J. Anal. Chem. 1995, 67, 735.
54. Hostetler, M. J.; Green, S. J.; Stokes, J. J.; Murray, R. W. J. Am. Chem. Soc. 1996, 118, 4212.
55. Nelles, G.; Schönherr, G.; Jaschke, M.; Wolf, H.; Schaub, M.; Küther, J.; Tremel, W.; Bamberg, E.; Ringsdorf, H.; Butt, H.-J. Langmuir 1998, 14, 808.
56. Weisbecker, C. S.; Merritt, M. V.; Whitesides, G. M. Langmuir 1996, 12, 3763.
57. The absorbance peak for the Au sol used in the modification study differs from those reported above (i.e., it is red-shifted compared with the 5- and 28-nm sols) because the average colloid size for this in-house prepared sol is larger.
58. Lee, P. C.; Meisel, D. J. Phys. Chem. 1982, 86, 3391.