An FTIR Study of Anhydride Formation on Heating Butane Tetracarboxylic Acid in the Presence of Various Catalysts

Textile Research Journal

Volumn 69, Issue 12, 1999, Pages 949-955

  Gillingham, Estelle L ^a   Lewis, David M ^a   Voncina, Bojana ^b  

^a UNIVERSITY OF LEEDS   (United Kingdom)

^b UNIVERSITY OF MARIBOR   (Slovenia)

Author keywords

[No Author keywords available]

Indexed keywords

CATALYST; COTTON; CROSS LINKING; POLYCARBOXYLIC ACID; SPECTROSCOPY; TEMPERATURE;

EID: 0033512563     PISSN: 00405175     EISSN: None     Source Type: Journal    
DOI: 10.1177/004051759906901211     Document Type: Article

References (25)

1. Andrews, B.A.K., and Morris, N.M., Alkali Metal Salts of Hydroxyl Acids as Catalyst in Durable Press Finishing with Butanetetracarboxylic Acid, J. Textile Inst. 84 (4), 631-637 (1993).
2. Andrews, B.A.K., Welch, C.M., and Trask-Morrell, B.J., Efficient Ester Crosslink Finishing for Formaldehyde-Free Durable Press Cotton Fabrics, Am. Dyest. Rep. 78 (6), 15-23 (1989).
3. Bellamy, L.J., “The Infra Red Spectra of Complex Molecules,” 3rd ed., Chapman and Hall, London, 1975, pp. 144-145.
4. Borune, E.J., Stacey, M., Tatlow, J.C., and Tedder, J.M., Studies on Trifluoroacetic Acid, Part 1: Trifluoroacetic Anhydride as a Promoter of Ester Formation between Hydroxy-compound and Carboxylic Acid, J. Chem. Soc. 2976-2979 (1949).
5. Brown, R.O., Reidsville, N.C., and Tomasino, C., Catalysis of 1,2,3,4-Butanetetracarboxylic Acid in the Durable Press Finishing of Cotton Textiles, in “Book of Papers, Amer. Assoc. of Text. Chem. And Color Int. Conference and Exhibition,” Charlotte, SC, Oct. 1991, pp. 168-185.
6. Gagliardi, D.D., and Shippee, F.B., Crosslinking of Cellulose with Polycarboxylic Acids, Am. Dyest. Rep. 52, 300-303 (1963).
7. Gillingham, E.L., Methods to Fix Polycarboxylated and Polyphosphonated Dyes onto Cellulosic Substrates, Doctoral dissertation, University of Leeds, U.K., 1995.
8. McConnell, B.L., Graham, L.A., and Swidler, R.A., A. New Reactive System for Continuous Dyeing and Printing of Cellulose and Blends, Textile Res. J. 49, 458-467 (1979).
9. Khorana, H.G., The Chemistry of Carbodiimides, Chem. Rev. 53, 145-166 (1953).
10. Khorana, H.G., and Todd, A.R., Studies on Phosphorylation, Part XI, J. Chem. Soc., 2257-2260 (1953).
11. Kurzer, F., and Douraghi-Zadeh, K., Advances in the Chemistry of Carbodiimides, Chem. Rev. 67 (2), 107-152 (1967).
12. Nkeonye, P.O., The Effect of Acid Liberating Salts on the Carboxylic Acid Dye-Cellulose Reaction, Textile Dyer Print. 24 (9), 29-31 (1991).
13. Rowland, S.P., Welch, C.M., Brannan, A.F., and Gallagher, D.M., Introduction of Ester Cross Links into Cotton Cellulose by a Rapid Curing Process, Textile Res. J. 37, 933-941 (1967).
14. Sandler, S.R., and Karo, W., “Organic Functional Group Preparation, vol III, Academic Press Inc., 1989.
15. Silverstein, R.M., Clayton Bassler, G., and Mortill, T.C., “Spectrometric Identification of Organic Compounds,” 3rd ed., John Wiley & Sons, NY, 1975, pp. 104, 151.
16. Voncina, B., Polycarboxylic Acids in Cellulose Cotton Dyeing and Finishing, Doctoral dissertation, University of Leeds, U.K., 1995.
17. Welch, C.M., Durable Press Finishing without Formaldehyde, Textile Chem. Color. 22 (5), 13-16 (1990).
18. Welch, C.M., Tetracarboxylic Acids as Formaldehyde-Free Durable Press Finishing Agents, Part I: Catylyst, Additive, and Durability Studies, Textile Res. J. 58, 480-486 (1988).
19. Welch, C.M., and Andrews, B.A.K., Ester Crosslinks: A Route to High Performance Nonformaldehyde Finishing of Cotton, Textile Chem. Color. 21 (2), 13-17 (1989).
20. Welch, C.M., and Peter, J.G., Mixed Polycarboxylic Acids and Mixed Catylyst in Formaldehyde-Free Durable Press Finishing, Textile Chem. Color. 29 (3), 22-27 (1997).
21. Yang, C.Q., FT-IR Spectroscopy Study of the Ester Crosslinking Mechanism of Cotton Cellulose, Textile Res. J. 61, 433-440 (1991).
22. Yang, C.Q., Infrared Spectroscopy Studies of the Cyclic Anhydride as the Intermediate for the Ester Crosslinking of Cotton Cellulose by Polycarboxylic Acids, I: Identification of the Cyclic Anhydride Intermediate, J. Polym. Sci. Part A Polym. Chem. 31, 1187-1193 (1993).
23. Yang, C.Q., and Wang, X., Infrared Spectroscopy Studies of the Cyclic Anhydride as the Intermediate for the Ester Crosslinking of Cotton Cellulose by Polycarboxylic Acids, II; Comparison of Different Polycarboxylic Acids, J. Polym. Sci. Part A Polym. Chem. 34, 1573-1580 (1996).
24. Yang, C.Q., and Wang, X., Infrared Spectroscopy Studies of the Cyclic Anhydride as the Intermediate for the Ester Crosslinking of Cotton Cellulose by Polycarboxylic Acids, III: The Molecular Weight of a Crosslinking Agent, J. Polym. Sci. Part A Polym. Chem. 35, 557-564 (1997).
25. Yang, C.Q., and Wang, X., Formation of the Cyclic Anhydride Reactive Intermediate and the Esterification of Cotton Cellulose by Multifunctional Carboxylic Acids: An Infrared Spectroscopy Study, Textile Res. J. 66, 595-603 (1996).