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85033963168
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note
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Compounds 5 and 25 did not dissolve in pure MeOH.
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24
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85033964717
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note
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Chemical shifts of the ring methine carbons are also highly indicative of ring size, i.e. THF carbon atoms are generally found 5-15 ppm downfield from those in 6-membered rings.
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27
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0009073551
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See also reference 15
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