Resolution of Spiro[4.4]nonane-1,6-dione by Chiral Inclusion Complexation

Chinese Chemical Letters

Volumn 10, Issue 7, 1999, Pages 559-562

  Feng, Xiao Ming ^a   Zeng, De Chao ^a   Li, Zhi ^a   Jiang, Yao Zhong ^a  

^a CHENGDU INSTITUTE OF ORGANIC CHEMISTRY   (China)

Author keywords

Chiral inclusion complexation; Enantioselectivity; Resolution

Indexed keywords

EID: 0033461396     PISSN: 10018417     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (8)

1. A. S. C. Chan, W. H. Hu, C. C. Pai, C. P. Lau, Y. Z. Jiang, A. Q. Mi, M. Yan, J. Sun, R. L. Lou, and J. G. Deng, J. Am. Chem. Soc., 1997, 119, 9570.
2. N. Harada, N. Ochiai, K. Takada, H. Uda, J. Chem. Soc., Chem. Commun., 1977, 495.
3. Y. Z. Jiang, M. Yan, J. Sun, W. H. Hu, Z. Li, A. Q. Mi, A. S. C. Chan, Chinese J. Chem., 1998, 16(3), 258.
4. X. M. Feng, D. C. Zeng, Y. Z. Jiang, Z. Li, CN 98 1 12086.5(Application No.).
5. F. Toda, J. Synth. Org. Chem., Jpn., 1994, 52(11), 923.
6. F. Toda. Acc. Chem. Res., 1995, 28, 480.
7. -1.
8. 3). Racemic spiro[4.4]nonane-1,6-dione: δ (ppm) 1.2-2.4 (12H,m). R-(+)-BINOL: δ (ppm) 5.07 (-OH,broad). Complex: 5.20 (-OH,sharp),