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For all of the homo-couplings described in the experimental section, Acros Cu(OAc)2 was employed.
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85033942207
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note
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1H} NMR (134.19 MHz) spectra were obtained on a Bruker WM 360-MHz multinuclear spectrometer. Reaction mixtures (in DMF) were referenced against internal tetramethyltin (TMT).
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35
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85033960745
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note
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4, followed by the evaporation of solvents.
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