Electrothermal atomization atomic absorption spectrometry for the determination of lead in urine: results of an interlaboratory study

Spectrochimica acta, Part B: Atomic spectroscopy

Volumn 54, Issue 5, 1999, Pages 853-864

  Parsons, Patrick J ^a,b   Slavin, Walter ^c  

^a WADSWORTH CENTER   (United States)

^b STATE UNIVERSITY OF NEW YORK   (United States)

^c Bonaire Technologies   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ATOMIZERS; BODY FLUIDS; CHEMICAL ANALYSIS; GAS CHROMATOGRAPHY; MASS SPECTROMETRY; QUALITY CONTROL; SPECTROMETRY;

ELECTROTHERMAL ATOMIZATION ATOMIC ABSORPTION SPECTROMETRY; FLAME ATOMIC ABSORPTION WITH EXTRACTION; INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY; ISOTOPE DILUTION; TRANSVERSE HEATED GRAPHITE ATOMIZER; URINE;

LEAD;

EID: 0033340675     PISSN: 05848547     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0584-8547(99)00007-5     Document Type: Article

References (21)

1. Centers for Disease Control, Screening Young Children for Lead Poisoning: Guidance for State and Local Public Health Officials [Report], US Department of Health and Human Services, Atlanta, GA, USA 1997.
2. National Committee for Clinical Laboratory Standards, Analytical Procedures for the Determination of Lead in Blood and Urine; Proposed Guideline., NCCLS Document C40-P Wayne, PA, 1998.
3. American Academy of Pediatrics Committee on Drugs: Treatment guidelines for lead exposure in children, Pediatrics 96 (1995) pp. 155-160.
4. Pleban P.A., Pearson K.H. Determination of lead in whole blood and urine using Zeeman-effect flameless atomic-absorption spectroscopy. Anal. Lett. 12:1979;935-950.
5. Legotte P.A., Rosa W.C., Sutton D.C. Determination of cadmium and lead in urine and other biological samples by graphite-furnace atomic-absorption spectrometry. Talanta. 27:1980;39-44.
6. Shan X.-q., Ni Z.-m. Matrix modification for the determination of lead in urine by graphite furnace atomic absorption spectrometry. Can. J. Spect. 27:1982;75-81.
7. Slavin W., Carnrick G.R., Manning D.C., Pruszkowska E. Recent experiences with the stabilized temperature platform furnace and Zeeman background correction. At. Spectrosc. 4:1983;69-86.
8. Subramanian K.S., Meranger J.C., MacKeen J.E. Graphite-furnace atomic-absorption spectrometry with matrix modification for determination of cadmium and lead in human urine. Anal. Chem. 55:1983;1064-1067.
9. Paschal D.C., Kimberly M.M. Determination of urinary lead by electrothermal atomic absorption with the stabilized-temperature platform furnace and matrix modification. At. Spectrosc. 6:1985;134-136.
10. Liang L. Direct determination of lead in urine by Zeeman atomic-absorption spectrometry with the stabilized-temperature-platform furnace. Spectrochim. Acta Part B. 41:1986;1131-1135.
11. D' Haese P.C., Lamberts L.V., Liang L., Van de Vyver F.L., De Broe M.E. Elimination of matrix and spectral interference in the measurement of lead and cadmium in urine and blood by electrothermal atomic-absorption spectrometry with deuterium background correction. Clin. Chem. 37:1991;1583-1588.
12. G. Sesana, A. Baj, Determination of lead and cadmium in urine using Zeeman GFAAS, in: C. Minoia, S. Caroli (Eds.), Applications of Zeeman Graphite Furnace Atomic Absorption Spectrometry in the Chemical Laboratory and in Toxicology, Pergamon Press, New York, 1992, pp. 459-474.
13. D.L. Tsalev, Atomic Absorption Spectroscopy in Occupational and Environmental Health Practice, vol. III, CRC Press, Boca Raton, 1995.
14. H.T. Delves, I.L. Shuttler, Elemental analysis of body fluids and tissues by electrothermal atomization and atomic absorption spectrometry, in: S.J. Haswell (Ed.), Atomic Absorption Spectrometry. Theory, Design and Applications, Elsevier, Amsterdam, 1991, Chapter 4k, p. 381.
15. Parsons P.J., Slavin W. A rapid Zeeman graphite furnace atomic absorption spectrometric method for the determination of lead in blood. Spectrochim. Acta Part B. 48:1993;925-939.
16. Aggarwal S.K., Kinter M., Herold D.A. Determination of lead in urine and whole blood by stable isotope dilution gas chromatography-mass spectrometry. Clin. Chem. 40:1994;1494-1502.
17. J.F. Tyson, R.I. Ellis, N.N. Ertas, S.A. McIntosh, F. Fernandez, Determination of Lead in Urine by Flow-injection Hydride-generation-atomic Absorption Spectrometry with Quartz Tube Atomization. Personal Communication, 1998.
18. Paschal D.C., Ting B.G., Morrow J.C., Pirkle J.L., Jackson R.J., Sampson E.J., Miller D.T. Trace metals in urine of United States residents: reference range concentrations. Environ. Res. 76:1998;53-59.
19. Zhang L., Carnrick G., Slavin W. Rapid analysis with transversely heated furnace atomic absorption spectroscopy. Spectrochim. Acta Part B. 48:1993;1435-1443.
20. Qiao H., Parsons P.J., Slavin W. Transferability of blood lead determinations by furnace atomic absorption spectrophotometry and continuum background correction. Clin. Chem. 41:1995;1451-1454.
21. C.E. Flajnik, D. Shrader, Determination of Lead in Urine by GFAAS-Deuterium and Zeeman Background Correction, Varian AA Technical Note June, 1993.