Construction of the tetranuclear complex with inter- and intramolecular stacking-like arrangement composed of planar palladium(II) units

Chemistry Letters

Volumn , Issue 4, 1999, Pages 315-316

  Yamada, Yasunori ^a   Okamoto, Ken Ichi ^a  

^a UNIVERSITY OF TSUKUBA   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0033245717     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.1999.315     Document Type: Article

References (14)

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8. sh.
9. -1 for MoKα radiation (λ = 0.71069 Å). Measurements were carried out on a Rigaku AFC7S diffractometer. The structure was solved by a direct method and refined by a full-matrix least square. Final R = 0.028 and Rw = 0.046 for 8217 observed reflections ( I > 2.00σ(I)). Selected bond distances (Å) and angles (°): Pd1-S1 = 2.2934(8), Pd1-S3 = 2.3023(9), Pd1-N1 = 2.094(3), Pd1-N2 = 2.073(3), Pd2-S2 = 2.2871(9), Pd2-S4 = 2.2872(9), Pd2-N3 = 2.085(3), Pd2-N4 = 2.091(3), Pd3-S1 = 2.2773(9), Pd3-S2 = 2.2832(9), Pd3-N5 = 2.066(3), Pd3-N6 = 2.079(3), Pd4-S3 = 2.2711(9), Pd1-S4 = 2.2620(9), Pd4-N7 = 2.066(3), Pd4-N8 = 2.086(3), S1-Pd1-S3 = 87.13(3), N1-Pd1-N2 = 79.5(1), S2-Pd2-S4 = 86.38(3), N3-Pd2-N4 = 79.1(1), S1-Pd3-S2 = 94.62(3), N5-Pd3-N6 = 93.0(1), S3-Pd4-S4 = 93.80(3), N7-Pd4-N8 = 93.9(1), Pd1-S1-Pd3 = 117.32(4), Pd2-S2-Pd3 = 111.12(4), Pd1-S3-Pd4 = 121.08(4), Pd2-S4-Pd4 = 112.46(4).
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