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-1): 3577(m), 3527(s), 3348(m), 3345(s), 3305(m), 3237(m), 3052(w), 2978(w), 1638(m), 1577(m), 1562(m), 1425(m), 1396(w), 1376(w), 1272(m), 1090(vs), 1012(m), 922(m), 783(w), 749(w), 625(s), 553(w).
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6
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0009197107
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3CN to give a light blue, easy dissolved in DMF giving a green solution.
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7
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2(F)] for 5001 observed reflections [ I > 2σ(I), 2θ < 50.1°]. Data were collected on an Enraf-Nonius CAD4 diffractometer using graphite-monochromated Mo-Kα radiation (λ = 0.71069 Å) and employing the ω-2θ scan method. The structure was solved by direct methods and successive Fourier difference synthesis and refined by full-matrix least-squares methods. Non-H atoms were inserted at their calculated positions and treated anisotropically. The C(14) atom in the ethanol group as solvent molecule showed large thermal parameters. H atoms were generated geometrically, but not refined. All calculations were performed on a MICRO VAX 3100 computer using the TEXSAN program package.
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