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Chemistry Letters

Volumn , Issue 10, 1999, Pages 1083-1084

The ruthenium-catalyzed addition of C-H bonds in aromatic nitriles to olefins

(5) Kakiuchi, Fumitoshi a Sonoda, Motohiro a Tsujimoto, Takuya a Chatani, Naoto a Murai, Shinji a

a OSAKA UNIVERSITY (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0033235147 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.1999.1083 Document Type: Article

Times cited : (88)

References (31)

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- note
- The similar catalytic coupling of acetophenone with the same olefin 2 gave a mixture of 1:1 and 1:2 adducts. As an exception, the catalytic reaction of acetophenone with trimethylvinylsilane gave 1:2 adduct predominately (Ref. 7b).

31
- 0009105470
- note
- 3 of toluene, o-tolunitrile (2 mmol), and triethoxyvinylsilane (1900 mg, 10 mmol). The mixture was heated under vigorous refluxing conditions (135 °C, oil bath temperature) with stirring. After heating for 48 h, the mixture was allowed to cool to room temperature, and toluene and unreacted triethoxyvinylsilane were removed by rotary evaporation (40 °C/5 mmHg, 1 mmHg = 133.322 Pa). The product was isolated by bulb-to-bulb distillation (120 °C/2 mmHg) in 78% yield. The GC yield of the product (86% yield) was determined in a separate run under the same reaction conditions described above except for the use of hexadecane as an internal standard for GC.

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