The structure of R-NiF3, and synthesis, and magnetism of new R3 MIINiIVF6 (M = Fe, Co, Cu, Zn), and MIINiIIF4 (M = Co, Cu)

Comptes Rendus de l'Academie des Sciences - Series IIc: Chemistry

Volumn 2, Issue 11-13, 1999, Pages 557-563

  Shen, Ciping ^a   Chacón, Lisa C ^a   Rosov, Nicholas ^b   Elder, Scott H ^a   Allman, John C ^a   Bartlett, Neil ^a  

^a UNIVERSITY OF CALIFORNIA   (United States)

^b NATIONAL INSTITUTE OF STANDARDS AND TECHNOLOGY   (United States)

Author keywords

Field dependent magnetic susceptibility; Metastability; Pseudo trifluorides; Room temperature preparations

Indexed keywords

EID: 0033229430     PISSN: 13871609     EISSN: None     Source Type: Journal    
DOI: 10.1016/S1387-1609(00)88566-7     Document Type: Article

References (25)

1. [1] Klemm W., Huss E., Z. anorg. allgem. Chemie 258 (1949) 221-226.
2. [2] Lucier G.M., Whalen J.M., Bartlett N., J. Fluor. Chem. 89 (1998) 101-104.
3. [3] Whalen J.M., Lucier G.M., Chacón L.C., Bartlett N., J. Fluor. Chem. 88 (1998) 107-110.
4. [4] Graudejus O., Elder S.H., Lucier G.M., Shen C., Bartlett N., Inorg. Chem. 38 (1999) 2503-2509.
5. [5] Zemva B., Lutar K., Jesih A., Casteel W.J. Jr., Wilkinson P., Cox D.E., Von Dreele R.B., Borrmann H., Bartlett, N. J. Amer. Chem. Soc. 113 (1991) 4192-4198.
6. [6] Zemva B., Lutar K., Chacón L., Fele-Buermann M., Allman J., Shen C., Bartlett N., J. Am. Chem. Soc. 117 (1995) 10025-10034.
7. [7] Bartlett N., Chambers R.D., Roche A.J., Spink R.C.H., Chacón L., Whalen J.M., Chem. Eng. Commun. (1996) 1049-1050; Whalen J.M., Chacón L., Bartlett N., Electrochem. Soc. Proceedings 97-15 (1997) 1-12.
8. [7] Bartlett N., Chambers R.D., Roche A.J., Spink R.C.H., Chacón L., Whalen J.M., Chem. Eng. Commun.(1996) 1049-1050; Whalen J.M., Chacón L., Bartlett N., Electrochem. Soc. Proceedings 97-15 (1997) 1-12.
9. [8] Zemva B., Hagiwara R., Casteel W.J. Jr., Lutar K., Jesih A., Bartlett N., J. Amer. Chem. Soc. 112 (1990) 4846-4849.
10. [9] Lutar K., Jesih A., Leban I., Zemva B., Bartlett N. Inorg. Chem. 28 (1989) 3467-3471.
11. [10] Casteel W.J. Jr., Lucier G., Hagiwara R., Borrmann H., Bartlett N., J. Solid State Chem. 96 (1992) 84-96.
12. [11] Christe K., Wilson W.W., Bougon R.A., Charpin P., J. Fluorine Chem. 34 (1987) 287-298.
13. [12] Siegel S., Gebert E., J. Am. Chem. Soc. 85 (1963) 240.
14. [13] Bartlett N., Rao P.R., Proc. Chem. Soc. (1964) 393-394.
15. [14] Tressaud A., Winteberger M., Bartlett N., Hagenmuller P., C. R. Acad. Sci. Paris, série C 282 (1976) 1069-1072.
16. [15]The neutron powder diffraction measurements were made with the high resolution powder diffractometer (BT-1) at the Reactor of the National Institute of Standards and Technology, Gaithersburg, MD. Samples for neutron powder diffraction were contained in a cylindrical aluminum sample container, which was 6.95 mm (i.d.), 9.0 mm (o.d.) and 31.8 mm long. The cap for the sample container was threaded and a seal was made with a Teflon o-ring which fitted into a groove on the container. The cap was hex-cut so as to facilitate tightening with a wrench. On top of the cap was a threaded connector, such that the sample container could be attached to the end of a pole which was inserted into a cryostat. The cryostat containing the sample was then positioned in the path of the neutron beam. Data were collected at several temperatures to ascertain if nuclear and/or magnetic phase transitions took place at low temperature. Structure solutions were achieved with the General Structure Analysis System (Larson A.C., Von Dreele R.B., Los Alamos Laboratory Report No. LA-UR-86-748, 1987). The Al container peaks were removed by Le Bail extraction. [Le Bail A., Duroy H., Fourquet J.-L., Mater. Res. Bull. 23 (1988) 447.]
17. [15]The neutron powder diffraction measurements were made with the high resolution powder diffractometer (BT-1) at the Reactor of the National Institute of Standards and Technology, Gaithersburg, MD. Samples for neutron powder diffraction were contained in a cylindrical aluminum sample container, which was 6.95 mm (i.d.), 9.0 mm (o.d.) and 31.8 mm long. The cap for the sample container was threaded and a seal was made with a Teflon o-ring which fitted into a groove on the container. The cap was hex-cut so as to facilitate tightening with a wrench. On top of the cap was a threaded connector, such that the sample container could be attached to the end of a pole which was inserted into a cryostat. The cryostat containing the sample was then positioned in the path of the neutron beam. Data were collected at several temperatures to ascertain if nuclear and/or magnetic phase transitions took place at low temperature. Structure solutions were achieved with the General Structure Analysis System (Larson A.C., Von Dreele R.B., Los Alamos Laboratory Report No. LA-UR-86-748, 1987). The Al container peaks were removed by Le Bail extraction. [Le Bail A., Duroy H., Fourquet J.-L., Mater. Res. Bull. 23 (1988) 447.]
18. [16] Baur W.H., Acta Cryst. 11 (1958) 488-490.
19. [17]Taylor J.C., Wilson P.W., J. Inorg. Nucl. Chem. 36(1974) 1561-1563.
20. [18] Babel D., Tressaud A., in: Hagenmuller P. (Ed.), Inorganic Solid fluorides, Academic Press Inc., New York, London, 1985, pp. 77-192.
21. [19] Tressaud A., Sherwood R.C., Bartlett N. to be published.
22. [20] Dance J-M., Tressaud A., in: Hagenmuller P. (Ed.), Inorganic Solid fluorides, Academic Press Inc., New York, London, 1985, pp. 371-391.
23. [21] Tressaud A., Parenteau J.-M., Dance J.-M., Portier J., Hagenmuller P., Mat. Res. Bull. 8 (1973) 565-570.
24. [22] Bizette H., J. Phys. Radium 12 (1951) 161-169; Bizette H., Tsai B., C. R. Acad. Sci. Paris 238 (1954) 1575-1576.
25. [22] Bizette H., J. Phys. Radium 12 (1951) 161-169; Bizette H., Tsai B., C. R. Acad. Sci. Paris 238 (1954) 1575-1576.