Determination of dexamethasone in bovine liver by chemiluminescence high-performance liquid chromatography

Journal of Agricultural and Food Chemistry

Volumn 47, Issue 10, 1999, Pages 4275-4279

  Iglesias, Y ^a   Fente, C A ^a   Vazquez B ^a   Franco, C ^a   Cepeda, A ^a   Mayo, S ^b   Gigosos, P G ^b  

^a UNIVERSITY OF SANTIAGO DE COMPOSTELA   (Spain)

^b Lab de Salud Publica de Lugo   (Spain)

Author keywords

Chemiluminescence; Dexamethasone; HPLC; Liver; Luminol

Indexed keywords

ANTIINFLAMMATORY AGENT; CORTICOSTEROID; DEXAMETHASONE; DRUG RESIDUE; REAGENT;

ANIMAL; ANIMAL TISSUE; ARTICLE; CATTLE; CHEMICAL STRUCTURE; CHEMISTRY; CHEMOLUMINESCENCE; CHROMATOGRAPHY; DRUG DETERMINATION; FOOD CONTROL; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; ISOLATION AND PURIFICATION; LIQUID LIQUID EXTRACTION; LIVER; METHODOLOGY; NONHUMAN; TISSUE DISTRIBUTION;

ANIMALS; ANTI-INFLAMMATORY AGENTS; CATTLE; CHEMILUMINESCENT MEASUREMENTS; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DEXAMETHASONE; DRUG RESIDUES; FOOD INSPECTION; HUMANS; LIVER;

ANIMALIA; BOS TAURUS; BOVINAE;

EID: 0033212894     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf990334b     Document Type: Article

References (19)

1. Amsterdamsky, C.; Aubry, J. M.; Panico, R. Bioluminescence et chimiluminescence. Actual. Chim. 1984, 31-39.
2. Baeyens, W.; Keukeleire, D.; Korkidis, K. Luminescence techniques in chemical and biochemical analysis; State University of Ghent: Belgium, 1991.
3. Calokerinos, A. C.; Deftereos, N. T.; Baeyens, W. Chemiluminescence in drug assay. J. Pharm. Biomed. Anal. 1995, 13, 1063-1071.
4. Code of Federal Regulations; U.S. Government Printing Office: Washington, DC, 1993; Title 21, Sections 520.540 and 522.540.
5. Ferguson, D. C.; Hoening, M. Glucocorticoids, mineralocorticoids, and steroid synthesis inhibitors. Endocrine Pharmacology. 1995, chapter 32.
6. Fiori, M.; Pierdominici, E.; Longo, F.; Brambilla, G. Identification of main corticosteroids as illegal feed additives in milk replacers by liquid chromatographic-atmospheric pressure chemical ionisation mass spectrometry. J. Chromatogr. 1998, 807, 219-227.
7. Ishida, J.; Sonezaki, S.; Yamaguchi, M. High-performance liquid chromatographic determination of 3α,5β-tetrahydroaldosterone in human urine with chemiluminescence detection. Analyst 1992, 117, 3-8.
8. Ishida, J.; Yamaguchi, M.; Nakahara, T.; Nakamura, M. 4,5-Diaminophthalhydrazide as a highly sensitive chemiluminescence reagent for α-keto acids in liquid chromatography. Anal. Chim. Acta 1990, 231, 1-6.
9. Kawasaki, T.; Maeda, M.; Tsuji, Akio. Determination of 17-oxoesteroids in serum and urine by fluorescence high-performance liquid chromatography using dansyl hydrazine as a pre-labeling reagent. J. Chromatogr. 1981, 226, 1-12.
10. Kayganich, K.; Watson, J. T.; Kilts, C.; Ritchie, J. Determination of plasma dexamethasone by chemical oxidation and electron capture negative ionization mass spectrometry. Biomed. Environ. Mass Spectrom. 1990, 19, 341-347.
11. Koziol, T.; Grayeski, M. L.; Weinberger, R. Determination of trace levels of steroids in blood plasma by liquid chromatography with peroxyoxalate chemiluminescence detection. J. Chromatogr. 1984, 317, 355-366.
12. Mallinson, E. T.; Dreas, J. S.; Wilson, R. T.; Henry, A. C. Determination of dexamethasone in liver and muscle by liquid chromatography and gas chromatography/mass spectrometry. J. Agric. Food Chem. 1995, 43, 140-145.
13. McLaughlin, L. G.; Henion, J. D. Determination of dexamethasone in bovine tissues by coupled-column normal-phase high-performance liquid chromatography and capillary gas chromatography-mass spectrometry. J. Chromatogr. 1990, 529, 1-19.
14. Nakamura, J.; Yakata, M. Determination of urinary cortisol and 6β-hydroxycortisol by high performance liquid chromatography. Clin. Chem. 1985, 149, 215-224.
15. Official Journal of the European Community; Annex to Council Directive 85/591/EEC.; Feb 12, 1989; Section 1.27, p L 351/ 42.
16. Official Journal of the European Community; Comission Reglament 749/97; April 25, 1997; p L 110/24.
17. Shearan, P.; O'Keeffe, M.; Smyth, M. R. Reversed-phase high-performance liquid chromatographic determination of dexamethasone in bovine tissues. Analyst 1991, 116, 1365-1368.
18. Takeda, M.; Maeda, M.; Tsuji, A. Chemiluminescence high performance liquid chromatography of corticosteroids using Lucigenin as post-column reagent. Biomed. Chromatogr. 1990, 4, 119-122.
19. Toriba, A.; Kubo, H. Chemiluminescence high performance liquid chromatography of corticosteroids and p-nitrophanacyl esters based on the luminol reaction. J. Liq. Chromatogr. Relat. Technol. 1997, 20 (18), 2965-2977