Analysis of metsulfuron-methyl in soil by liquid chromatography/tandem mass spectrometry. Application to a field dissipation study

Journal of Agricultural and Food Chemistry

Volumn 47, Issue 10, 1999, Pages 4462-4468

  Bossi, Rossana ^a   Seiden, Piet ^b   Andersen, Søren M ^c   Jacobsen, Carsten S ^c   Streibig, Jens C ^b  

^a NATIONAL ENVIRONMENTAL RESEARCH INSTITUTE   (Denmark)

^b UNIVERSITY OF COPENHAGEN   (Denmark)

^c GEOLOGICAL SURVEY OF DENMARK AND GREENLAND   (Denmark)

Author keywords

ESI LC MS MS; Field dissipation; Metsulfuron methyl; Microbial degradation; Mineralization; Triazine amine

Indexed keywords

ARYLSULFONIC ACID DERIVATIVE; CARBON 14; HERBICIDE; METSULFURON METHYL; PESTICIDE RESIDUE; SULFONAMIDE; SULFONYLUREA DERIVATIVE; TRIAZINE DERIVATIVE;

ANALYTIC METHOD; ARTICLE; AUTOCLAVE; BARLEY; CONTROLLED STUDY; DEGRADATION; HALF LIFE TIME; ISOLATION AND PURIFICATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; MINERALIZATION; PESTICIDE SPRAYING; POLLUTANT; SOIL; SOIL TREATMENT; TANDEM MASS SPECTROMETRY; TIME;

ARYLSULFONATES; CHROMATOGRAPHY, LIQUID; ENVIRONMENTAL POLLUTANTS; HERBICIDES; MASS SPECTROMETRY; PESTICIDE RESIDUES; SOIL; TIME FACTORS;

HORDEUM VULGARE SUBSP. VULGARE;

EID: 0033212841     PISSN: 00218561     EISSN: None     Source Type: Journal    
DOI: 10.1021/jf981280t     Document Type: Article

References (35)

1. Bastide, J.; Badon, R.; Cambon, J. P.; Vega, D. Transformation rates of ortho-substituted thiophene and benzene carboxylic esters: application to thifensulfuron-methyl and metsulfuron-methyl herbicides. Pestic. Sci. 1994, 40, 293-297.
2. Berdeaux, O.; De Alencastro, L. F.; Grandjean, D.; Tarradellas, J. Supercritical fluid extraction of sulfonylurea herbicides in soil samples. Int. J. Environ. Anal. Chem. 1994, 56, 109-117.
3. Berger, B. M.; Wolfe, N. L. Hydrolysis and biodegradation of sulfonylurea herbicides in aqueous buffers and anaerobic water-sediment systems: assessing fate pathways using molecular descriptors. Environ. Toxicol. Chem. 1996, 15, 1500-1507.
4. Bernal, J. L.; Jimenéz, J. J.; Herguedas, A.; Atienza, J. Determination of chlorsulfuron and tribenuron-methyl residues in agricultural soils. J. Chromatogr. 1998, 778, 119-125.
5. Beyer, E. M., Jr.; Duffy, M. J.; Hay, J. V.; Schlueter, D. D. Sulfonylureas. In Herbicides: Chemistry, Degradation and Mode of Action; Kearny, P. C., Kaufman, D. D., Eds.; Dekker: New York, 1988; Chapter 3, pp 117-189.
6. Boldt, T. S.; Jacobsen, C. S. Different toxic effects of the sulfonylurea herbicides metsulfuron-methyl, chlorsulfuron and thifensulfuron-methyl on fluorescent Pseudomonas isolated from an agricultural soil. FEMS Microbiol. Lett. 1998, 29-35.
7. Bossi, R.; Køppen, B.; Spliid, N. H.; Streibig, J. C. Analysis of sulfonylurea herbicides in soil water at sub-ppb levels by electrospray negative ionization-mass spectrometry followed by confirmatory tandem MS-MS. J. AOAC Int. 1998, 81, 775-784.
8. Bray, L. D.; Heard, N. E.; Overman, M. C.; Vargo, J. D.; King, D. L.; Lawrence, L. J.; Phelps, A. W Hydrolysis of prosulfuron at pH 5: evidence for a resonance-stabilized triazine cleavage product. Pestic. Sci. 1997, 51, 56-64.
9. Cambon, J.-P.; Bastide, J. Hydrolysis kinetics of thifensulfuron methyl in aqueous buffer solutions. J. Agric. Food Chem. 1996, 44, 333-337.
10. Cook, A. M.; Hütter, R. s-Triazines as nitrogen sources for bacteria. J. Agric. Food Chem. 1981, 29, 1135-1143.
11. Dinelli, G.; Vicari, A.; Brandolini, V. Detection and quantitation of sulfonylurea herbicides in soil at the ppb level by capillary electrophoresis. J. Chromatogr. 1995, 700, 201-207.
12. Font, N.; Hernández, F.; Hogendoorn, E. A.; Baumann, R. A.; van Zoonen, P. Microwave-assisted solvent extraction and reversed-phase liquid chromatography-UV detection for screening soils for sulfonylurea herbicides. J. Chromatogr. 1998, 798, 179-186.
13. Galletti, G. C.; Bonetti, A.; Dinelli, G. High-performance liquid chromatography determination of sulfonylureas in soil and water. J. Chromatogr. 1995, 692, 27-37.
14. Gould, W. D.; Hagedorn, C.; Bardinelli, T. R.; Zablotowicz, R. M. New selective media for enumeration and recovery of fluorescent Pseudomonas from various habitats. Appl. Environ. Microbiol. 1985, 49, 28-32.
15. Hemmamda, S.; Calmon, M.; Calmon, J. P. Kinetics and hydrolysis mechanism of chlorsulfuron and metsulfuronmethyl. Pestic. Sci. 1994, 40, 71-76.
16. Klaffenbach, P.; Holland, P. T. Analysis of sulfonylurea herbicides by gas-liquid chromatography. Determination of chlorsulfuron and metsulfuron-methyl in soil and water samples. J. Agric. Food Chem. 1993, 41, 396-401.
17. Li, L. Y. T.; Campbell, D. A.; Bennet, P. K; Henion, J. Acceptance criteria for ultratrace HPLC-tandem mass spectrometry: quantitative and qualitative determination of sulfonylurea herbicides in soil. Anal. Chem. 1996, 68, 3397-3404.
18. Mandelbaum, R. T.; Allan, D. L.; Wackett, L. P. Isolation and characterization of a Pseudomonas sp. that mineralizes the s-triazine herbicide atrazine. Appl. Environ. Microbiol. 1995, 61, 1451-1457.
19. Marek, L. J.; Koskinen, W. LC/MS analysis of 4-methoxy-6-methyl-1,3,5-triazin-2-yl-containing sulfonylurea herbicides in soil. J. Agric. Food Chem. 1996, 44, 3878-3881.
20. Nord-Christenson, M.; Bergstöm, L. Field observation of soil movement and residues of sulfonylureas in Sweden. Proceedings of the Brighton Crop Protection Conference-Weeds 3; BCPC: Farnham, U.K., 1989; pp 1127-1132.
21. Powley, C. R.; de Bernard, P. A. Screening method for nine sulfonylurea herbicides in soil and water by liquid chromatography with ultraviolet detection. J. Agric. Food Chem. 1998, 46, 514-519.
22. Radosevich, M.; Traina, S. J.; Hao, Y.-L.; Tuovinen, O. H. Degradation and mineralization of atrazine by a soil bacterial isolate. Appl. Environ. Microbiol. 1995, 61, 297-302
23. Robinson, R. C.; Dunham, R. J. The uptake of soil-applied chlorotriazines by seedlings and its prediction. Weed Res. 1982, 22, 223-236.
24. Sabadie, J. Hydrolyse chimique acide du metsulfuron méthyle. Weed Res. 1990, 30, 413-419.
25. Sabadie, J. Dégradation du chlorsulfuron et du metsulfuron méthyle en présence d'acides humiques. Weed Res. 1993, 33, 397-407.
26. Streibig, J. C.; Walker, A.; Blair, A. M.; Anderson-Taylor, G.; Eagle, D. J.; Friedländer, H.; Hacker, E.; Iwanzik, W.; Kudsk, P.; Labhart, C.; Luscombe, B. M.; Madafiglio, G.; Nel, P. C.; Pestemer, W.; Rahman, A.; Retzlaff, G.; Rola, J.; Stefanovic, L.; Straathof, H. J.; Thies, E. P. Variability of bioassay with metsulfuron-methyl in soil. Weed Res. 1995, 35, 214-224.
27. Strek, H. J. Fate of chlorsulfuron in the environment. Laboratory evaluations. Pestic. Sci. 1998, 53, 29-51.
28. Vega, D.; Bastide, J.; Poulain, C. Dégradation chimique ou microbiologique des sulfonylurées dans le sol. II. Cas du metsulfuron méthyle. Weed Res. 1992, 32, 149-155.
29. Vicari, A.; Catizone, P.; Zimdahl, R. L. Persistence and mobility of chlorsulfuron and metsulfuron under different soil and climatic conditions. Weed Res. 1894, 34, 147-155.
30. Wadd, D. J.; Drennan, D. S. H. A field study of the persistence and leaching of chlorsulfuron and metsulfuron-methyl. Proceedings of the Brighton Crop Protection Conference - Weeds 3; BCPC: Franham, U.K., 1989; pp 1133-1138.
31. Walker, A.; Welch, S. J. The relative movement and persistence in soil of chlorsulfuron, metsulfuron-methyl and triasulfuron. Weed Res. 1989, 29, 375-383.
32. Walker, A.; Cotterill, E. G.; Welch, S. J. Adsorption and degradation of chlorsulfuron and metsulfuron-methyl in soils from different depths. Weed Res. 1989, 29, 281-287.
33. Willems, H. P. L.; Lewis, K. J.; Dyson, J. S.; Lewis, F. J. Soil Biol. Biochem. 1996, 28, 989-996.
34. Young, M. S. Preparation of environmental samples for determination of sulfonylurea herbicides by solid-phase extraction using a polymeric sorbent. J. AOAC Int. 1998, 81, 99-104.
35. Zahnow, E. W. Analysis of the herbicide sulfometuron methyl in soil and water by liquid chromatography. J. Agric. Food Chem. 1985, 33, 479-483.