Isotropic Mixing, Sign Discrimination, and Sensitivity in Solid-State Wideline Heteronuclear Correlation Experiments

Journal of Magnetic Resonance

Volumn 140, Issue 1, 1999, Pages 235-241

  Oliver, Sarah L ^a   Titman, Jeremy J ^a  

^a UNIVERSITY OF NOTTINGHAM   (United Kingdom)

Author keywords

Heteronuclear correlation experiments; Isotropic mixing; Semicrystalline polymers; Sensitivity; Spin diffusion

Indexed keywords

CARBON; POLYETHYLENE;

ARTICLE; CHEMISTRY; CRYSTALLIZATION; FOURIER ANALYSIS; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SENSITIVITY AND SPECIFICITY; THEORETICAL MODEL;

CARBON ISOTOPES; CRYSTALLIZATION; FOURIER ANALYSIS; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, THEORETICAL; POLYETHYLENE; SENSITIVITY AND SPECIFICITY;

EID: 0033185658     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.1999.1844     Document Type: Article

References (23)

1. P. Caravatti, L. Braunschweiler, and R. R. Ernst, Chem. Phys. Lett. 100, 305 (1983); D. P. Burum and A. Bielecki, J. Magn. Reson. 94, 645 (1991).
2. P. Caravatti, L. Braunschweiler, and R. R. Ernst, Chem. Phys. Lett. 100, 305 (1983); D. P. Burum and A. Bielecki, J. Magn. Reson. 94, 645 (1991).
3. S. Kaplan, Macromolecules 26, 1060 (1993); J. L. White and P. Mirau, Macromolecules 27, 1648 (1994); S. Li, D. M. Rice, and F. E. Karasz, Macromolecules 27, 2211 (1994); J. L White, A. J. Dias, and J. R. Ashbaugh, Macromolecules 31, 1880 (1998); J. L White and P. Brant, Macromolecules 31, 5424 (1998).
4. S. Kaplan, Macromolecules 26, 1060 (1993); J. L. White and P. Mirau, Macromolecules 27, 1648 (1994); S. Li, D. M. Rice, and F. E. Karasz, Macromolecules 27, 2211 (1994); J. L White, A. J. Dias, and J. R. Ashbaugh, Macromolecules 31, 1880 (1998); J. L White and P. Brant, Macromolecules 31, 5424 (1998).
5. S. Kaplan, Macromolecules 26, 1060 (1993); J. L. White and P. Mirau, Macromolecules 27, 1648 (1994); S. Li, D. M. Rice, and F. E. Karasz, Macromolecules 27, 2211 (1994); J. L White, A. J. Dias, and J. R. Ashbaugh, Macromolecules 31, 1880 (1998); J. L White and P. Brant, Macromolecules 31, 5424 (1998).
6. S. Kaplan, Macromolecules 26, 1060 (1993); J. L. White and P. Mirau, Macromolecules 27, 1648 (1994); S. Li, D. M. Rice, and F. E. Karasz, Macromolecules 27, 2211 (1994); J. L White, A. J. Dias, and J. R. Ashbaugh, Macromolecules 31, 1880 (1998); J. L White and P. Brant, Macromolecules 31, 5424 (1998).
7. S. Kaplan, Macromolecules 26, 1060 (1993); J. L. White and P. Mirau, Macromolecules 27, 1648 (1994); S. Li, D. M. Rice, and F. E. Karasz, Macromolecules 27, 2211 (1994); J. L White, A. J. Dias, and J. R. Ashbaugh, Macromolecules 31, 1880 (1998); J. L White and P. Brant, Macromolecules 31, 5424 (1998).
8. C. B. Lee and R. G. Griffin, Biophys. J. 55, 355 (1989).
9. Z. T. Gu, C. F. Ridenour, C. E. Bronnimann, T. Iwashita, and A. McDermott, J. Am. Chem. Soc. 118, 822 (1996).
10. B. J. van Rossum, G. J. Boender, and H. J. M. de Groot, J. Magn. Reson. 120, 274 (1996); B. J. van Rossum, H. Forster, and H. J. M. de Groot, J. Magn. Reson. 124, 516 (1997).
11. B. J. van Rossum, G. J. Boender, and H. J. M. de Groot, J. Magn. Reson. 120, 274 (1996); B. J. van Rossum, H. Forster, and H. J. M. de Groot, J. Magn. Reson. 124, 516 (1997).
12. K. Schmidt-Rohr, J. Clauss, and H. W. Spiess, Macromolecules 25, 3273 (1992); J. Clauss, K. Schmidt-Rohr, A. Adam, C. Boeffel, and H. W. Spiess, Macromolecules 25, 5208 (1992).
13. K. Schmidt-Rohr, J. Clauss, and H. W. Spiess, Macromolecules 25, 3273 (1992); J. Clauss, K. Schmidt-Rohr, A. Adam, C. Boeffel, and H. W. Spiess, Macromolecules 25, 5208 (1992).
14. P. Caravatti, G. Bodenhausen, and R. R. Ernst, Chem. Phys. Lett. 89, 363 (1982).
15. A. Kubo and C. A. McDowell, J. Magn. Reson. 100, 517 (1992).
16. J. Cavanagh and M. Rance, Annu. Rep. NMR Spectrosc. 27, 1 (1993).
17. A. E. Tonelli, "NMR Spectroscopy and Polymer Microstructure," VCH, New York (1989).
18. D. J. States, R. A. Haberkorn, and D. J. Ruben, J. Magn. Reson. 48, 286 (1983).
19. L. Braunschweiler and R. R. Ernst, J. Magn. Reson. 53, 521 (1983).
20. D. P. Burum, M. Linder, and R. R. Ernst, J. Magn. Reson. 44, 173 (1981).
21. H. W. Spiess, in "NMR Basic Principles and Progress" (P. Diehl, E. Fluck, and R. Kosfeld, Eds.), Springer, Berlin (1978).
22. H. Geen, J. J. Titman, and H. W. Spiess, Chem. Phys. Lett. 213, 145 (1993).
23. M. Baldus and B. H. Meier, J. Magn. Reson. 121, 65 (1996).