Continuous synthesis of TiO2 fine particles and increase of particle size using a two-stage slug flow tubular reactor

Chemical Engineering Research and Design

Volumn 77, Issue 4, 1999, Pages 335-341

  Kubo, M ^a   Yonemoto, T ^a  

^a TOHOKU UNIVERSITY   (Japan)

Author keywords

Continuous synthesis; Mathematical model; Slug flow; Titanium dioxide; Two stage

Indexed keywords

CHEMICAL REACTORS; MATHEMATICAL MODELS; PARTICLE SIZE ANALYSIS; SYNTHESIS (CHEMICAL); WATER;

CONTINUOUS SYNTHESIS; GEOMETRIC STANDARD DEVIATION (GSD); SLUG FLOW TUBULAR REACTORS;

TITANIUM DIOXIDE;

PARTICLE; REACTOR; SLUG FLOW; TITANIUM DIOXIDE;

EID: 0033150798     PISSN: 02638762     EISSN: None     Source Type: Journal    
DOI: 10.1205/026387699526278     Document Type: Article

References (27)

1. Chen, S., Dong, P., Yang, G. H. and Yang, J. J., 1996, Kinetics of formation of monodisperse colloidal silica particles through the hydrolysis and condensation of tetraethlorthosilicate, Ind Eng Chem Res, 35: 4487-4493.
2. Yoldas, B. E., 1973, Hydrolysis of aluminum alkoxides and bayerite conversion, J Appl Chem Biotechnol, 23: 803-809.
3. Harris, M. T., Brunson, R. R. and Byers, C. H., 1990, The base-catalyzed hydrolysis and condensation reactions of dilute and concentrated TEOS solutions, J Non-Cryst Solids, 121: 397-403.
4. Bailey, J. K. and Macartney, M. L., 1992, Formation of colloidal silica particles from alkoxides, Colloids Surfaces, 63: 151-161.
5. 5 powders, J Mater Sci, 21: 2771-2774.
6. 5 powder, J Mater Sci, 25: 1013-1017.
7. 2 powder, J Am Ceram Soc, 65: C199-C201.
8. 4, J Ceram Soc Jpn, 93: 261-266.
9. 2 powders generated with HPC dispersant, J Am Ceram Soc, 65: 1574-1577.
10. 2 particles, J Am Ceram Soc, 72: 421-426.
11. Lerot, L., Legrand, F. and de Bruycker, P., 1991, Chemical control in precipitation of spherical zirconia particles, J Mater Sci, 26: 2353-2358.
12. Ogihara, T., Ikeda, M., Kato, M. and Mizutani, N., 1989, Continuous processing of monodispersed titania powders, J Am Ceram Soc, 72: 1598-1601.
13. Ogihara, T., Iizuka, M., Yamagawa, T, Ogata, N, and Yoshida, K, 1992, Continuous reactor system of monosized colloidal particles, J Mater Sci, 27: 55-62.
14. Ogihara, T., Yabuuchi, M., Yamagawa, T, Ogata, N, Yoshida, K, Nagata, N., Ogawa, K. and Maeda, U., 1997, Preparation of monodispersed spherical ferric oxide particles hydrolysis of metal alkoxides using a continuous tube-type reactor, Advanced Powder Technol, 8: 73-84.
15. Yonemoto, T., Kubo, M. Doi, T. and Tadaki, T., 1997, Continuous synthesis of titanium dioxide fine particles using a slug flow ageing tube reactor, Chem Eng Res Des Trans IChemE, Part A 75: 413-419.
16. Ogihara, T., Nakajima, H., Yanagawa, T., Ogata, N., Yoshida, K. and Matsushita, N., 1991, Preparation of monodisperse, spherical alumina powders from alkoxides, J Am Ceram Soc, 74: 2263-2269.
17. Stöber, W., Fink, A. and Bohn, E., 1968, Controlled growth of monodisperse silica spheres in the micron size range, J Colloid Interface Sci, 26: 62-69.
18. 4, Kagaku Kougaku Ronbunsyu, 18: 887-893.
19. Bogush, G. H., Tracy, M. H. and Zukoski, C. F., 1988, Preparation of monodispersed silica particles : Control of size and mass fraction, J Non-Crystalline Solids, 104: 95-106.
20. Hasegawa, M., Kimata, M. Ishibashi, S. and Kanda, Y., 1995, Preparation of monodisperse composite particles by hydrolysis of metal alkoxides with seed particles, Kagaku Kougaku Ronbunsyu, 21: 879-885.
21. 2 powders from alcohol solution, Langmuir, 2: 251-255.
22. Kumazawa, H., Hori, Y. and Sada, E., 1993, Synthesis of spherical zirconia fine particles by controlled hydrolysis of zirconium tetrabut-oxide in 1-propanol, Chem Eng J, 51: 129-133.
23. 2 particles using slug flow tubular reactor, Chem Eng Res Des Trans IChemE Part A, 76: 669-676.
24. 2 powders by hydrolysis of titanium tetraethoxide. 1. Synthesis and physical properties, Langmuir, 1: 414-420.
25. 2 powders, Am Ceram Soc Bull, 66: 1517-1520.
26. Higashitani, K. and Ishimura, K., 1997, Evaluation of interaction forces between surfaces in electrolyte solutions by atomic force microscope, J Chem Eng Jap, 30: 52-58.
27. Kanda, Y., Nakamura, T. and Higashitani, K., 1998, AFM studies of interaction forces between surfaces in alcohol-water solutions, Colloid Surface, 139: 55-62.