Synthesis and properties of dimethoxy-substituted unsymmetrical TTF derivatives

Synthetic Metals

Volumn 102, Issue 1-3, 1999, Pages 1693-1694

  Nishikawa, H ^a,c   Misaki, Y ^a   Yamabe, T ^a   Shiro, M ^b  

^a KYOTO UNIVERSITY   (Japan)

^b RIGAKU CORPORATION   (Japan)

^c TOKYO METROPOLITAN UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

CRYSTAL STRUCTURE; CYCLIC VOLTAMMETRY; ELECTRIC CONDUCTIVITY; ELECTROCHEMISTRY; SYNTHESIS (CHEMICAL); VAN DER WAALS FORCES; X RAY CRYSTALLOGRAPHY;

COUPLING REACTION; TETRATHIAFULVALENE;

ORGANIC CONDUCTORS;

EID: 0033137625     PISSN: 03796779     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0379-6779(98)00609-2     Document Type: Article

References (12)

1. T. Suzuki, H. Yamochi, G. Srdanov, K. Hinkelmann, and F. Wudl, J. Am. Chem. Soc. 111 (1989) 3108.
2. M. A. Beno, H. H. Wang, A. M. Kini, K. D. Carlson, U. Geiser, W. K. Kwok, J. E. Thompson, J. M. Williams, J. Ren, and M.-H. Whangbo, Inorg. Chem. 29 (1990) 159 9;
3. S. Kahlich, D. Schweitzer, I. Meinen, S. E. Lan, B. J. Nuber, H. Keller, K. Winzer H. W. Heiberg, Solid State Commun. 80 (1990) 191.
4. T. Mori, H. Inokuchi, A. M. Kini, J. M. Williams, Chem. Lett. 1990, 1297;
5. G. C. Papavassiliou, V. C. Kakoussis, D. J. Lagouvardos, G. A. Mousdis, Mol. Cryst. Liq. Cryst. 181 (1990) 171.
6. Y. Misaki, H. Nishikawa, K. Nomura, T. Yamabe, H. Yamochi, G. Saito, T. Sato, M. Shiro, J. Chem. Soc. Chem. Commun. (1992) 1410.
7. K. Kikuchi, M. Kikuchi, T. Namiki, K. Saito, I. Ikemoto, K. Murata, T. Ishiguro K. Kobayashi, Chem. Lett (1987), 931; G. C. Papavassiliou, G. A. Mousdis J. S. Zambounis, Synth. Met. 27 (1988) B379; Y. Misaki, N. Higuchi, H. Fujiwara, T. Yamabe, T. Mori, H. Mori, S. Tanaka, Angew. Chem. Int. Ed. Engl. 34 (1995) 1222.
8. K. Kikuchi, M. Kikuchi, T. Namiki, K. Saito, I. Ikemoto, K. Murata, T. Ishiguro K. Kobayashi, Chem. Lett (1987), 931; G. C. Papavassiliou, G. A. Mousdis J. S. Zambounis, Synth. Met. 27 (1988) B379; Y. Misaki, N. Higuchi, H. Fujiwara, T. Yamabe, T. Mori, H. Mori, S. Tanaka, Angew. Chem. Int. Ed. Engl. 34 (1995) 1222.
9. K. Kikuchi, M. Kikuchi, T. Namiki, K. Saito, I. Ikemoto, K. Murata, T. Ishiguro K. Kobayashi, Chem. Lett (1987), 931; G. C. Papavassiliou, G. A. Mousdis J. S. Zambounis, Synth. Met. 27 (1988) B379; Y. Misaki, N. Higuchi, H. Fujiwara, T. Yamabe, T. Mori, H. Mori, S. Tanaka, Angew. Chem. Int. Ed. Engl. 34 (1995) 1222.
10. 2a: 13% yield, 2b: 24%, 2c: 19%, 2d: 28%, 2e: 22%, 2f: 13%.
11. The redox potentials of 7 measured under the identical conditions with 2. 7a: +0.84, +1.13 V (vs. SCE); 7b: +0.51, +0.78 V; 7c: +0.50, +0.72 V; 7d: +0.51, +0.82 V; 7e: +0.52, +0.83 V; 7f: +0.42, +0.73 V.
12. w = 0.058 for 1362 observed ([I ≥ 3σ(I)]) reflections from 1989 unique data.